FAPAS YETERLİK TESTLERİ PROGRAMI. Nisan 2012 Mart 2013

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1 FAPAS YETERLİK TESTLERİ PROGRAMI Lütfen açıklamaları okuyunuz. Nisan 2012 Mart 2013 FAPAS Programını Program sayfalarında inceleyebilirsiniz. Notlar a) İlginizi çekebilecek testleri daha kolay bulabilmeniz için indeks sayfasını kullanabilirsiniz. b) Belirtilen dağıtım tarihleri planlanan tarihlerdir. Kayıt yaptıdırdığınız testlerden, herhangi bir sebeple ertelenenler olduğu takdirde ile tarafınıza bildirilecektir. Testlerin büyük bir bölümünün kapanış tarihleri dağıtım tarihlerinden itibaren 6-8 haftadır. c) Her test için test materyallerinin yaklaşık miktarları verilmiştir. Metodunuz daha fazla materyal gerektiriyorsa lütfen ekstra test materyal sayısını bildiriniz. İlave test materyaller için ücret ödenir. d) Ekstra test materyalleri ilave performans değerlendirmesi hakkı kazandırmaz. Birden fazla değerlendirme için çoklu kayıt yaptırmanız gerekmektedir. e) Test materyalleri DHL ile gönderilir. Kayıtlar: FAPAS Programına kayıtlar için Fera Standard Terms and Conditions for Proficiency Testing Schemes dokümanında belirtilen şartlar geçerlidir. Dokümana adresinden ulaşılabilir. Notlar a) 30 gün içerisinde kayıt onayınız ulaşmazsa lütfen iletişime geçiniz. b) Siparişiniz alındığında faturanız kesilecektir. Bu, ödemelerin testlerden önce yapılacağı anlamına gelmektedir. İlave notlar: i. Dağıtım a) Yukarıda da belirtildiği gibi, numuneler DHL ile gönderilmektedir. Bazı paketler sıcaklık değişimlerini minimize etmek için buz bloklar içerir ancak soğuk araçlarda taşınmamaktadır. Numuneniz elinize ulaştığında sıcaklığı yüksek de olsa, taşıma süresinin büyük bölümünde soğuk kaldığından dolayı testler için uygundur. b) Numuneniz dağıtımdan itibaren 4 gün içerisinde elinize ulaşmadığında lütfen iletişime geçiniz. c) Numuneler gönderildiğinde, kayıtlı olan adresine FAPAS tarafından DHL takip numarası Airway Bill Number gönderilecektir. d) Takip numaralarına kullanıcı adı ve şifrenizle girdiğiniz FAPAS web sitesindeki sayfanızdan da ulaşabilirsiniz. e) Numunelerin takibi katılımcı sorumluluğundadır. ii. Gümrük a) Test materyallerinin gümrüklerdeki muhtemel hasar ve kayıplarından veya olası gümrük işlemlerinden FAPAS sorumlu değildir. iii. Sonuçlar a) Katılımcıların sonuçları bildirmesi için numune dağıtım tarihinden itibaren genellikle 6 haftaları bulunmaktadır. Bazı analizler test materyali ve/veya analitlerden kaynaklanan nedenlerden dolayı daha kısa sürede tamamlanmalıdır. Bu testler programda belirtilmektedir. b) Sonuçlar FAPAS web sitesi üzerinden kabul edilmektedir. iv. Raporlar a) Test fiyatlarına katılımcıların kullanıcı adı şifreleriyle giriş yaptığı sistemde görebileceği elektronik rapor dahildir. b) Raporlar genellikle testin kapanmasından 5 hafta sonra web sitesinde yayımlanır. c) Raporlar PDF formatında ve dijital imzalı olarak sunulmaktadır. Görüntülemek için Adobe Reader 7 veya üzeri gerekmektedir.

2 Index FAPAS YETERLİK TESTLERİ PROGRAMI 3-MCPD & 1,3 DCP... 2 acesulfame-k acidity acrylamide... 2 aflatoxins... 9 alcoholic strength almond... 7, 9 almond protein... 7 aluminium animal (pork) fat animal feed... 9, 10 anisidine value anthelmintics... 4, 5 antimony antioxidants apple juice... 10, 13 apple purée... 10, 17 apricot purée arsenic arsenic, inorganic ash... 1, 6 aspartame avermectins... 4, 5 barley flour beef... 3 benzoic acid... 11, 13 beta-agonists... 4 beta-lactams... 4, 5 biscuits... 2 bisphenol A... 8 bovine milk... 5 bovine muscle... 4 bovine urine... 5 brandy bread... 1 breadcrumbs... 1 breakfast cereal... 8, 10, 11 brix... 11, 13 butyric acid... 1, 14 cabbage purée... 3, 17 cadmium caffeine... 11, 13 cake mix... 6, 7 calcium... 6, 8, 13 canned fish... 6, 7 canned meat... 1, 8 canned meat meal... 1 cephalosporins... 5 cereal... 1, 9, 10, 14, 16 cheese... 1 chicken... 3 chicken muscle... 5 chilli powder... 9, 12 chilli sugar paste chloramphenicol... 4, 5 chloride... 1, 11 chlormequat Nisan 2012 Mart 2013 chocolate... 1, 6, 7 chocolate cake mix cholesterol chromium citric acid... 11, 13 coccidiostats... 4, 5 cocoa... 10, 12 cola drink colours condensed milk... 1 copper... 6, 12 corn/maize... 1 corned beef... 4 crab meat cranberry juice crispbread... 2 crude fibre... 6 cyanuric acid... 2 cyclamate dairy ration... 6 deoxynivalenol (DON) diastase... 2 dihydrostreptomycin... 5 DON... 9 dried apricot dried figs... 9 dried vine fruit edible oil egg... 7 egg, egg white protein... 6 eggs... 5 ELISA... 6, 7, 9 energy drink... 8 esters of 3-MCPD... 2 ethyl acetate ethyl carbamate fatty acids fish... 1, 3, 4, 6, 12, 14 fish identification... 3 fish muscle... 4 fish oil fish paste... 1 fluoroquinolones... 4, 5 food simulant... 8 formaldehyde... 8 fructose... 2, 13 fruit juice fruit purée fumonisins... 9, 10 ginger (spice)... 9 glucose... 2, 13 gluten... 6, 7 grape purée grapefruit juice green bean (inc pods) purée green coffee ground coffee FAPAS (Index) Rev: Sayfa 1 / 2 hazelnut (water/nut slurry)... 9 hazelnut, hazelnut protein... 7 higher alcohols (sum)...13 histamine... 6, 7 honey... 2, 4, 5 hot pepper sauce...11 hydrogenated vegetable oil...15 hydroxymethylfurfural (HMF)... 2 hydroxyproline... 1 illegal dyes...11 immersion in ethanol... 8 immersion in olive oil... 8 infant cereal...12 infant formula... 12, 14 infant soya formula... 6 instant coffee...10 iodine... 8, 14 iodine value...14 iron... 6, 8, 12 jam... 7, 11 k232 & k lactose... 1 lamb... 3 LC-PUFAs...14 lead... 6, 12 lemon purée...17 lettuce purée... 3, 17 leucomalachite green... 4 liquid vitamin supplement...11 magesium... 6 magnesium... 6, 8, 13 maize... 9 maize flour... 10, 16 manganese... 6, 8 meat... 3, 11 melamine... 2, 8 melon purée...17 mercury...12 mercury, methyl...12 methanol...13 methylbutanol...13 milk... 6, 7 milk powder... 2, 3, 8, 9, 11, 12, 15 mixed fat spread...14 moisture... 1, 2, 6 molybdenum...12 nitrate... 3 nitrite... 3 nitrofuran metabolites... 5 nitrofurans... 4, 5 nitrogen... 1 non-fat solids... 1 non-permitted colours...11 NSAIDs... 4, 5 NSP fibre... 1 nut contamination... 7 nutritionally fortified oil...14

3 FAPAS YETERLİK TESTLERİ PROGRAMI Nisan 2012 Mart 2013 nylon film... 8 oat flour ochratoxin A oil... 8, 11 oily fish olive oil...7, 8, 14, 15 omega-3 & omega orange juice orange purée OTA... 9 overall migration... 8 PAHs... 7 PAHs (EU priority)... 7 palm oil... 7 paprika patulin peanut... 6, 9 peanut, peanut protein... 6 pear purée penicillins... 5 permitted colours peroxide value pesticide residues... 15, 16, 17, 18 ph... 11, 13 phosphoric acid (as P 2O 5) phosphorus... 6, 8, 13 photo initiators... 8 phthlates... 8 pig kidney... 4 pig liver... 4 pig ration... 6 pistachio (water/nut slurry)... 9 plastic film... 8 pork... 3 porridge oats... 1 potassium... 8, 13 potato purée poultry ration... 6 powdered baby food powdered rice prawns... 4, 5 premix... 6 protein... 6 quinine quinolones... 4, 5 quinolones & fluoroquinolones... 4, 5 refined palm oil... 2 rice... 9 rice (brown) roasted coffee saccharin saturated FAs selenium... 6, 8, 12 sheep feed... 6 smoked meat... 7 snack food... 1 sodium... 1, 6, 11, 13 soft drink... 12, 13 sorbic acid... 11, 13 soy sauce... 2 soya flour soya, soya protein... 7 spinach purée... 3 starch... 1, 6 strawberry purée sucrose... 2, 11, 13 sugar confectionary sulfonamides... 4, 5 sulphites... 6, 7 sulphur dioxide sweet (bell) pepper purée synthetic hormones... 4, 5 T-2 & HT-2 toxins tea tetracyclines... 4, 5 theobromine thyrostats... 4, 5 tin...12 titratable acidity... 1 tomato paste...12 tomato purée...17 tomato sauce...11 tonic water...13 total acidity... 11, 13 total dietary fibre... 1 total fat... 1, 14 total folate...11 total malachite green... 4 total niacin...11 total oil... 6 total primary aromatic amines... 8 total SO total sugars... 1, 6, 11, 13 total volatile basic nitrogen (TVB-N). 1 trans fatty acids...14 trifluralin (single herbicide)...15 TVB-Nitrogen... 1 unsaturated FAs, mono...14 unsaturated FAs, poly...14 vegetable oil...14 vegetable purée...12 veterinary drug residues... 4, 5 vine fruit...17 vitamins... 6, 11 volatile acidity...13 wheat flour... 1, 7, 10, 16 whisky...13 wine... 10, 12, 13 zearalenone (ZON)...10 zinc... 6, 8, 12 ZON... 9 β-agonists... 4, 5 FAPAS (Index) Rev: Sayfa 2 / 2

4 Besin Bileşenleri 12/04/ canned meat moisture, ash, total fat, nitrogen, sodium & chloride 1 13/06/ canned meat meal moisture, ash, total fat, nitrogen, sodium & chloride 1 23/08/ canned meat moisture, ash, total fat, nitrogen, hydroxyproline 1 17/10/ canned meat moisture, ash, total fat, nitrogen, hydroxyproline 1 04/01/ canned meat meal moisture, ash, total fat, nitrogen, sodium, chloride, total sugars 1 27/02/ canned meat moisture, ash, total fat, nitrogen, sodium, chloride 1 02/05/ wheat flour moisture at 130C, ash, nitrogen & total dietary fibre by AOAC 1 07/06/ porridge oats moisture at 130C, ash, total fat, nitrogen, total dietary fibre by AOAC & NSP fibre by Englyst 1 16/08/ bread sodium, 27/09/ cereal moisture at 130 o C, ash, nitrogen & total dietary fibre by AOAC 1 31/01/ breadcrumbs moisture, ash, nitrogen, starch & total dietary fibre by AOAC 1 24/05/ corn/maize snack food moisture, ash, total fat, nitrogen, sodium & chloride 03/07/ fish paste moisture, ash, total fat, nitrogen, sodium & chloride 1 01/08/ canned fish total volatile basic nitrogen (TVB-N) 1 30/08/ condensed milk moisture, ash, total fat, nitrogen & total sugars 150 ml 29/10/ chocolate moisture, total fat, butyric acid, lactose & sucrose 1 16/11/ milk powder moisture, ash, total fat, nitrogen, titratable acidity & lactose 25/01/ infant formula moisture, ash, total fat, nitrogen & lactose 13/02/ cheese & pasta meal moisture, ash, total fat, nitrogen, sodium & chloride 100 g 26/02/ butter moisture, total fat, non-fat solids, ph & chloride 200 g 20/03/ canned fish total volatile basic nitrogen (TVB-N) 1 Dipnotlar total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa, fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı. Sayfa 1 / 18

5 Acrylamide / Melamine / 3-MCPD 18/04/ milk powder melamine & cyanuric acid (low levels, <5 mg/kg) 10/07/ crispbread acrylamide 26/09/ animal feed melamine & cyanuric acid 19/10/ biscuits acrylamide 21/02/ milk powder melamine and cyanuric acid (> 5mg/kg) 25/05/ soy sauce 3-MCPD & 1,3 DCP 40 g 20/09/ refined palm oil esters of 3-MCPD 50 ml 09/01/ hydrolysed vegetable protein 3-MCPD & 1,3 DCP 40 g 14/03/ soy sauce 3-MCPD & 1,3 DCP 40 g Bal 17/07/ honey moisture, fructose, glucose, sucrose, hydroxymethylfurfural (HMF) & diastase 100 g 15/01/ honey a fructose, glucose, sucrose, hydroxymethylfurfural (HMF) & diastase 100 g Dipnotlar a bu test materyali tağşişli bal olabilir. Sayfa 2 / 18

6 Authenticity 13/04/ D chicken adulteration/contamination (presence/absence) of matrix with one or more from: beef, lamb or pork 19/07/ D lamb adulteration/contamination (presence/absence) of matrix with one or more from: beef, chicken or pork 18/09/ fish identification of unknown fish (3 samples) selected from the following list: Gadus morhua, (Linnaeus 1758) Limanda limanda, (Linnaeus 1758) Melanogrammus aeglefinus, (Linnaeus 1758) Merluccius merluccius, (Linnaeus 1758) Hippoglossus hippoglossus, (Linnaeus 1758) Pleuronectes platessa, (Linnaeus 1758) Pollachius virens, (Linnaeus 1758) Merlangius merlangus, (Linnaeus 1758) 04/12/ processed food adulteration/contamination (presence/absence) of matrix (2 samples) with pork 15/02/ D beef adulteration/contamination (presence/absence) of matrix with one or more from: chicken, lamb or pork 30 g 30 g 3 x 10 g 2 x 30 g 30 g Nitrate & Nitrite 25/04/ meat nitrate & nitrite 25 g 18/06/ cabbage purée nitrate 70 g 13/08/ lettuce purée nitrate 70 g 12/10/ milk powder nitrate & nitrite (low level) 40 g 16/11/ meat nitrate & nitrite 25 g 24/01/ feeding stuff nitrite 40 g 12/02/ spinach purée nitrate 70 g 25/03/ meat nitrate & nitrite 25 g D dondurarak kurutulmuş (freeze dried) numune, analizden önce tekrar sulandırılmalıdır. testin süresi kısadır Sayfa 3 / 18

7 Veteriner İlaç Kalıntıları 16/04/ fish muscle leucomalachite green & total malachite green 20 g 01/05/ # honey tetracyclines 20 g 15/05/ prawns chloramphenicol 20 g 29/05/ # pig kidney sulfonamides 20 g 25/06/ # fish muscle quinolones & fluoroquinolones 20 g 09/07/ # corned beef avermectins 20 g 30/07/ # pig liver β-agonists 20 g 06/08/ honey chloramphenicol 20 g 20/08/ # bovine muscle tetracyclines 20 g 04/09/ fish muscle (oily fish) leucomalachite green & total malachite green 20 g Dipnotlar # test Liste A'da belirtilen analitlerin belirlenmesi ve miktar tayinlerini içerir. testin süresi kısadır. Testlerde belirtilen genel kategorilerdeki muhtemel ilaç kalıntılarının listesi - Liste A. tetracyclines chlortetracycline (total), doxycycline, oxytetracycline (total), tetracycline (total) nitrofurans AHD (bound), AHD (total), AOZ (bound), AOZ (total), AMOZ (bound), AMOZ (total), SEM (bound), SEM (total) sulfonamides sulfachloropyridazine, sulfadiazine, sulfadimethoxine, sulfadimidine (sulfamethazine), sulfadoxine, sulfaguanadine, sulfamerazine, sulfamethizole, sulfamethoxazole, sulfamethoxypyridazine, sulfamonomethoxine, sulfamoxole, sulphanilamide, sulfapyridine, sulfaquinoxaline, sulfathiazole, sulfisoxazole quinolones & fluoroquinolones flumequine, nalidixic acid, oxolinic acid, ciprofloxacin, danofloxacin, difloxacin, enrofloxacin, marbofloxacin, norfloxacin, sarafloxacin avermectins abamectin, doramectin, emamectin, eprinomectin, ivermectin, moxidectin β-agonists bromobuterol, cimaterol, cimbuterol, clenbuterol, clenpenterol, hydroxyclenbuterol, mabuterol, mapenterol, ractopamine, salbutamol, salmeterol, terbutaline, tulobuterol, zilpaterol synthetic hormones α-boldenone, methylboldenone, diethylstilbestrol (DES), dienestrol, hexoestrol, methyltestosterone, α-nortestosterone, stanozolol, 16β-hydroxystanozolol, trenbolone, zeranol nonsteroidal anti-inflammatory diclofenac, 5-hydroxyflunixin, ibuprofen, meloxicam, naproxen, phenylbutazone drugs (NSAIDs) coccidiostats decoquinate,diclazuril, halofuginone, lasalocid, maduramycin, monensin, narasin, DNC, robenidine, salinomycin, semduramycin, toltrazuril sulfone anthelmintics albendazole sulfone, albendazole-2-amino-sulfone, albendazole sulfoxide, total albendazole sulfone, closantel, fenbantel, fenbendazole, oxfendazole, oxfendazole sulfone, total oxfendazole sulfone, flubendazole, levamisole, mebendazole, hydroxymebendazole, mebendazole amine, total mebendazole, nitroxynil, thiabendazole, triclabendazole, triclabendazole sulfone, triclalbendazole sulfoxide, ketotriclabendazole, total triclabendazole sulfone thyrostats 6-methyl-2-thiouracil, dimethylthiouracil, ethylthiouracil, methimazole, mercaptobenzimidazole, tapazole, thiouracil, methylthiouracil, phenylthiouracil, propylthiouracil beta-lactams amoxicillin, ampicillin, benzylpenicillin (Penicillin G), Penicillin V, cloxacillin, dicloxacillin, nafpicillin, oxacillin, cefalexin, cefalonium, cefapirin, desacetylcefapirin, cefazolin cefoperazone, cefquinome Sayfa 4 / 18

8 Veteriner İlaç Kalıntıları (devam) 25/09/ # honey sulfonamides 20 g 08/10/ # bovine milk NSAIDs (nonsteroidal anti-inflammatory drugs) 20 ml 30/10/ # chicken muscle coccidiostats 20 g 06/11/ # chicken eggs nitrofuran metabolites 20 g 27/11/ # bovine urine synthetic hormones & thyrostats 25 ml 08/01/ # chicken eggs quinolones & fluoroquinolones 20 g 29/01/ # prawns nitrofuran metabolites 20 g 11/02/ bovine milk chloramphenicol & thiamphenicol 20 ml 05/03/ # bovine milk anthelmintics 20 ml 26/03/ # bovine milk beta-lactams (penicillins & cephalosporins) & dihydrostreptomycin 40 ml Dipnotlar # test Liste A'da belirtilen analitlerin belirlenmesi ve miktar tayinlerini içerir. testin süresi kısadır. Testlerde belirtilen genel kategorilerdeki muhtemel ilaç kalıntılarının listesi - Liste A. tetracyclines chlortetracycline (total), doxycycline, oxytetracycline (total), tetracycline (total) nitrofurans AHD (bound), AHD (total), AOZ (bound), AOZ (total), AMOZ (bound), AMOZ (total), SEM (bound), SEM (total) sulfonamides sulfachloropyridazine, sulfadiazine, sulfadimethoxine, sulfadimidine (sulfamethazine), sulfadoxine, sulfaguanadine, sulfamerazine, sulfamethizole, sulfamethoxazole, sulfamethoxypyridazine, sulfamonomethoxine, sulfamoxole, sulphanilamide, sulfapyridine, sulfaquinoxaline, sulfathiazole, sulfisoxazole quinolones & fluoroquinolones flumequine, nalidixic acid, oxolinic acid, ciprofloxacin, danofloxacin, difloxacin, enrofloxacin, marbofloxacin, norfloxacin, sarafloxacin avermectins abamectin, doramectin, emamectin, eprinomectin, ivermectin, moxidectin β-agonists bromobuterol, cimaterol, cimbuterol, clenbuterol, clenpenterol, hydroxyclenbuterol, mabuterol, mapenterol, ractopamine, salbutamol, salmeterol, terbutaline, tulobuterol, zilpaterol synthetic hormones α-boldenone, methylboldenone, diethylstilbestrol (DES), dienestrol, hexoestrol, methyltestosterone, α-nortestosterone, stanozolol, 16β-hydroxystanozolol, trenbolone, zeranol nonsteroidal anti-inflammatory diclofenac, 5-hydroxyflunixin, ibuprofen, meloxicam, naproxen, phenylbutazone drugs (NSAIDs) coccidiostats decoquinate,diclazuril, halofuginone, lasalocid, maduramycin, monensin, narasin, DNC, robenidine, salinomycin, semduramycin, toltrazuril sulfone anthelmintics albendazole sulfone, albendazole-2-amino-sulfone, albendazole sulfoxide, total albendazole sulfone, closantel, fenbantel, fenbendazole, oxfendazole, oxfendazole sulfone, total oxfendazole sulfone, flubendazole, levamisole, mebendazole, hydroxymebendazole, mebendazole amine, total mebendazole, nitroxynil, thiabendazole, triclabendazole, triclabendazole sulfone, triclalbendazole sulfoxide, ketotriclabendazole, total triclabendazole sulfone thyrostats 6-methyl-2-thiouracil, dimethylthiouracil, ethylthiouracil, methimazole, mercaptobenzimidazole, tapazole, thiouracil, methylthiouracil, phenylthiouracil, propylthiouracil beta-lactams amoxicillin, ampicillin, benzylpenicillin (Penicillin G), Penicillin V, cloxacillin, dicloxacillin, nafpicillin, oxacillin, cefalexin, cefalonium, cefapirin, desacetylcefapirin, cefazolin cefoperazone, cefquinome Sayfa 5 / 18

9 Yem Maddeleri Yem maddeleri ile ilgili 04197, 04204, 04207, 17120, 2288, 2289, 2291 ve 3036 testlerinin de bulunduğunu dikkate alınız. 17/05/ dairy ration moisture, ash, total oil, protein & crude fibre 1 17/05/ dairy ration iron, lead, magnesium, manganese & selenium 1 28/06/ sheep feed moisture, ash, total oil, protein & copper 1 06/09/ pig ration moisture, ash, total oil, protein, crude fibre, vitamin E & zinc 1 09/11/ poultry ration moisture, ash, total oil, protein & crude fibre 1 09/11/ poultry ration starch, total sugars, calcium & phosphorus 1 14/02/ premix calcium, manganese, magnesium, phosphorus, sodium & zinc 1 14/02/ premix vitamin A, D 3, E 1 Allerjenler Histamin ve sülfitler DIŞINDA (genellikle HPLC metotları kullanılır), sonuçlar ELISA kitlerinin markasına göre gruplandırılarak değerlendirilir. 13/04/ infant soya formula milk 2 x 20 g 03/05/ cake mix egg, egg white protein 2 x 20 g 30/05/ canned fish histamine (high level) 145 g 27/06/ infant soya formula gluten 2 x 20 g 27/07/ chocolate peanut, peanut protein 2 x 20 g 02/08/ infant soya formula milk 2 x 20 g 24/08/ cake mix gluten 2 x 20 g 05/09/ canned fish histamine (low level) 145 g Dipnotlar total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa, fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı. iki adet test materyali gönderilir. Kalitatif ve kantitatif sonuçlar bildirilebilir. Kalitatif ve kantitatif sonuçlar bildirilebilir. /continued Sayfa 6 / 18

10 Allerjenler (devam) Histamin ve sülfitler DIŞINDA (genellikle HPLC metotları kullanılır), sonuçlar ELISA kitlerinin markasına göre gruplandırılarak değerlendirilir. 21/09/ chocolate hazelnut, hazelnut protein 2 x 20 g 23/10/ jam sulphites 20 g 31/10/ cake mix gluten, milk and egg 30 g 21/11/ wheat flour soya, soya protein 2 x 20 g 02/01/ chocolate contamination (presence/absence) of matrix with one or more from the following list: Almond, (Amygdalus communis L.) Hazelnut, (Corylus avellana) Walnut, (Juglans regia) Cashew, (Anacardium occidentale) Pecan nut, (Carya illinoiesis (Wangenh.) K. Koch)) Brazil nut, (Bertholletia excels) Pistachio nut, (Pistacia vera) Macadamia / Queensland nut (Macadamia ternifolia) 07/02/ canned fish histamine (high level) 145 g 07/03/ chocolate almond, almond protein 2 x 20 g Çevresel Bulaşanlar 20/04/ palm oil PAHs 30 ml 02/10/ smoked meat product PAHs 07/02/ olive oil all 16 EU priority PAHs 30 ml Dipnotlar iki adet test materyali gönderilir. Kalitatif ve kantitatif sonuçlar bildirilebilir. Kalitatif ve kantitatif sonuçlar bildirilebilir. sadece kalitatif sonuçlar Sayfa 7 / 18

11 Migrasyon Overall & Specific 26/04/ nylon film overall migration into ethanol by total immersion 40 cm x 22 cm 08/11/ plastic film overall migration into olive oil by total immersion 40 cm x 22 cm 21/06/ B food stimulant (oil) 19/07/ food simulant (3% w/v acetic acid in water) 15/08/ food simulant (50% w/v ethanol) 06/09/ food stimulant (3% w/v acetic acid in water) 23/11/ food simulant (3% w/v acetic acid in water) 28/02/ B food stimulant (oil) Besin Elementleri phthalates melamine bisphenol A formaldehyde total primary aromatic amines photo initiators 2 x 50 ml 50 ml 50 ml 50 ml >300 ml 2 x 50 ml 04/04/ canned meat calcium, phosphorus & zinc (all natural levels) 1 05/07/ breakfast cereal calcium, iron & zinc (fortified) 14/11/ milk powder calcium, iodine & selenium (all natural levels) 22/02/ energy drink iron, magnesium, manganese, potassium, selenium (all natural levels) Dipnotlar B Blank matriks dahildir. Sayfa 8 / 18

12 Mikotoksinler Aflatoksin 04192, 04201, ve ELISA taramaları yapan laboratuvarlara yöneliktir. 11/04/ maize aflatoxin B 1, DON, ZON & OTA 1 24/04/ pistachio (water/nut slurry) aflatoxins B & G &/or total 10/05/ maize aflatoxins B & G &/or total 55 g 18/05/ milk powder aflatoxin M 1 55 g 20/06/ chilli powder aflatoxins B & G &/or total 55 g 04/07/ animal feed (cereal based) aflatoxins B & G &/or total 25/07/ peanut aflatoxins B & G &/or total 55 g 07/08/ infant food contamination of matrix with one or more from the following list: aflatoxins B & G &/or total, OTA, ZON, DON, FB 1 & FB 2 & total fumonisins (as a sum of FB 1 & FB 2) 21/08/ almond (water/nut slurry) aflatoxins B & G &/or total 100 g 55 g g 07/09/ maize aflatoxin B 1, DON, ZON & OTA 1 26/09/ milk powder aflatoxin M 1 55 g 16/10/ hazelnut (water/nut slurry) 24/10/ animal feed (cereal based) aflatoxins B & G &/or total contamination of matrix with one or more from the following list: aflatoxin B 1, OTA, ZON & DON 07/11/ maize aflatoxins B & G &/or total 55 g 28/11/ mixed spice aflatoxins B & G &/or total 55 g 07/12/ animal feed (cereal based) 08/01/ pistachio (water/nut slurry) aflatoxins B & G &/or total aflatoxins B & G &/or total 100 g 1 55 g 100 g 23/01/ maize aflatoxin B 1, DON, ZON & OTA 1 31/01/ rice aflatoxins B & G &/or total 55 g 08/02/ peanut aflatoxins B & G &/or total 55 g 25/02/ dried figs (water/fruit slurry) aflatoxins B & G &/or total 100 g 23/03/ milk powder aflatoxin M 1 55 g Sayfa 9 / 18

13 Mikotoksinler Patulin 19/06/ apple juice (clear) patulin 50 ml 18/09/ apple purée patulin 60 g 19/02/ apple juice (cloudy) patulin Mikotoksinler Okratoksin A OTA ile ilgili 04199, 04201, ve roundlarının da bulunduğunu dikkate alınız. 50 ml 04/05/ wheat flour ochratoxin A 55 g 29/05/ dried vine fruit (water/fruit slurry) ochratoxin A 06/07/ barley flour ochratoxin A 55 g 09/08/ green coffee ochratoxin A 55 g 13/09/ paprika ochratoxin A 55 g 26/10/ instant coffee ochratoxin A 55 g 100 g 04/12/ wine ochratoxin A 55 ml 10/01/ maize flour ochratoxin A 55 g 08/02/ roasted coffee ochratoxin A 55 g 28/02/ animal feed ochratoxin A 55 g 21/03/ cocoa ochratoxin A 55 g Mikotoksinler Fusarium toksinleri Fusarium toksinleri içerebilecek 4199, 04201, ve roundlarının olduğunu da dikkate alınız. 18/04/ maize flour deoxynivalenol (DON) 55 g 06/06/ breakfast cereal zearalenone (ZON) 55 g 06/06/ breakfast cereal deoxynivalenol (DON) 55 g 28/06/ oat flour T-2 & HT-2 toxins 55 g 18/07/ maize flour FB 1 & FB 2 and total fumonisins (as a sum of FB 1 & FB 2) 55 g 01/11/ animal feed zearalenone (ZON) 55 g 01/11/ animal feed deoxynivalenol (DON) 55 g 30/01/ wheat flour deoxynivalenol (DON) 55 g 08/03/ animal feed T-2 & HT-2 toxins 55 g Sayfa 10 / 18

14 Vitaminler 24/05/ breakfast cereal vitamins B 1, B 2 (total) & B 6, total niacin & total folate 13/07/ fruit purée vitamin C 100 ml 20/11/ liquid vitamin supplement vitamins B 1, B 2 (total) & B 6 40 ml 17/01/ milk powder vitamins A & D 3 13/03/ powdered baby food vitamins A, B 12, C & E Bileşen / Katkı maddeleri 04/04/ tomato sauce brix, ph, total acidity, sodium & chloride 1 08/05/ meat sulphur dioxide 100 g 01/06/ jam brix, ph, benzoic acid, citric acid & sorbic acid 08/08/ chocolate cake mix caffeine, sorbic acid, theobromine & total sugars (expressed as sucrose) 11/09/ dried apricot (water/fruit slurry) sulphur dioxide 100 g 17/10/ sugar confectionary (boiled sweets) permitted colours up to 4 selected from the following list: Allura Red, Brilliant Blue FCF, Carmoisine, Erythrosine, Green S, Indigo Carmine, Patent Blue V, Ponceau 4R, Quinoline Yellow, Sunset Yellow FCF, Tartrazine 05/12/ oil antioxidants: total BHA (E320), BHT (E321) & propyl gallate (E310) 50 ml 20/02/ hot pepper sauce (or similar) non-permitted colours (illegal dyes) up to 4 selected from the following list: Butter Yellow (Dimethyl Yellow), Orange II, Para Red, Rhodamine B, Sudan I, Sudan II, Sudan III, Sudan IV, Sudan Black B, Sudan Orange G, Sudan Red B, Sudan Red 7B, Sudan Red G, Toluidine Red 50 ml Dipnotlar total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa, fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı. testin süresi kısadır. Kalitatif ve kantitatif sonuçlar bildirilebilir Sayfa 11 / 18

15 Metalik Bulaşanlar 19/04/ milk powder arsenic, cadmium, mercury & lead (all natural / low levels) 16/05/ soft drink antimony, arsenic (total) cadmium, chromium copper & zinc (all high levels) 14/06/ canned fish arsenic (total), cadmium & mercury (total) (all natural levels) 26/06/ tomato paste cadmium, lead, iron & tin (all high levels) 18/07/ chilli powder arsenic (total), cadmium & lead (all high levels) 03/08/ infant formula aluminium, chromium, molybdenum, selenium (all natural / low levels) 29/08/ canned crab meat arsenic (total), arsenic (inorganic), cadmium, lead & mercury (total) (all natural levels) 50 ml 19/09/ chilli sugar paste lead 25 g 28/09/ edible oil arsenic (total), copper, iron & lead (all high levels) ml 04/10/ wine ph, cadmium & lead 50 ml 25/10/ canned fish arsenic (total), cadmium, mercury (total) (all natural levels) 21/11/ infant cereal cadmium, chromium, lead, mercury (total) & selenium (all natural / low levels) 11/12/ soya flour aluminium, arsenic (total), cadmium, lead & mercury (total) (all high levels) 16/01/ cocoa powder cadmium & lead (both natural levels) 1 05/02/ fruit juice cadmium, iron, lead, & tin (all high levels) 50 ml 20/02/ powdered rice arsenic (inorganic), arsenic (total) & cadmium (all high levels) 19/03/ vegetable purée cadmium, lead & tin (all high levels) 27/03/ canned fish arsenic (total), methyl mercury & mercury (total) (all natural levels) 1 Sayfa 12 / 18

16 Meyve Suyu, Alkollü ve Alkolsüz İçecekler 31/05/ apple juice brix, ph, total acidity, total sugars, magnesium, potassium & sodium 11/10/ orange juice brix, ph, citric acid, sucrose, glucose, fructose & total sugars 03/01/ grapefruit juice brix, ph, total acidity, total sugars, calcium, magnesium & potassium 14/03/ cranberry juice brix, ph, total acidity, total sugars, phosphorus & potassium 250 ml 250 ml 250 ml 250 ml 04/05/ cola drink benzoic acid, caffeine, acesulfame-k & saccharin 12/07/ ground coffee caffeine (2 test materials supplied, one regular, one decaffeinated) 22/08/ soft drink brix, ph, citric acid, sorbic acid, cyclamate & saccharin 10/10/ soft drink up to 4 colours from the following list: Allura Red, Brilliant Blue FCF, Carmoisine, Erythrosine, Green S, Indigo Carmine, Patent Blue V, Ponceau 4R, Quinoline Yellow, Sunset Yellow FCF, Tartrazine 29/11/ cola drink caffeine, benzoic acid, total sugars & phosphoric acid (as P 2O 5) 13/02/ tonic water benzoic acid, quinine, acesulfame-k & aspartame 10/05/ whisky alcoholic strength, ethanol (acetaldehyde), ethyl acetate, methanol, propan-1-ol, 2-methylpropanol & 2-methylbutanol + 3-methylbutanol (sum) 12/09/ brandy alcoholic strength, ethanol (acetaldehyde), ethyl acetate, methanol, propan-1-ol, 2-methylpropanol & 2-methylbutanol + 3-methylbutanol (sum) & ethyl carbamate 06/02/ wine alcoholic strength, total SO 2, total acidity & volatile acidity 150 ml 2 x 30 g 150 ml 150 ml 150 ml 150 ml 200 ml 200 ml 220 ml Footnotes Dipnotlar total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa, fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı. Kalitatif ve kantitatif sonuçlar bildirilebilir. Sayfa 13 / 18

17 Sıvı ve Katı Yağlar 17/04/ nutritionally fortified oil (may contain LC-PUFAs) 09/05/ infant formula (may contain encapsulated LC-PUFAs) saturates, mono-unsaturates, poly-unsaturates, total trans fatty acids & individual fatty acids total fat, saturates, mono-unsaturates, poly-unsaturates, total trans fatty acids & individual fatty acids 30 ml 22/05/ olive oil peroxide value, acidity, anisidine value & iodine value 100 ml 11/07/ cereal product (may contain encapsulated LC-PUFAs) total fat, saturates, mono-unsaturates, poly-unsaturates, total trans fatty acids & individual fatty acids 27/07/ vegetable oil saturates, mono-unsaturates, poly-unsaturates & total trans fatty acids (& possibly individually specified fatty acids) 14/08/ mixed fat spread total fat, saturates, mono-unsaturates, poly-unsaturates, & trans fatty acids 09/10/ olive oil peroxide value, acidity, anisidine value & iodine value 30 ml 100 ml 18/10/ fish oil omega-3 & omega-6 series fatty acids 30 ml 27/11/ mixed fat spread total fat, butyric acid & cholesterol 06/02/ vegetable oil saturates, mono-unsaturates, poly-unsaturates 30 ml 11/03/ olive oil peroxide value, acidity, K 232 & K ml Dipnotlar testin süresi kısadır. Sayfa 14 / 18

18 Pestisit Kalıntıkları Hayvansal Ürünler / Katı ve Sıvı Yağlar Her test materyali (0588 hariç) Liste 1 de belirtilen pestisitlerden birkaç tanesini içerir. 25/04/ hydrogenated vegetable oil selection from List 1 25 g 0582b blank hydrogenated vegetable oil BLANK (only available if ordered with test 0582) 23/05/ milk powder selection from List 1 20/07/ olive oil selection from List 1 20/09/ hydrogenated vegetable oil 0585b blank hydrogenated vegetable oil selection from List 1 BLANK (only available if ordered with test 0585) 13/11/ oily fish selection from List 1 22/01/ animal (pork) fat selection from List 1 12/03/ fish muscle trifluralin (single herbicide) 20 g Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) Liste 1 aldrin cypermethrin fenpropimorph haloxyfop quintozene azinphos-ethyl pp-dde fenthion cis-heptachlor epoxide prochloraz bifenthrin pp-ddd (TDE) fenthion sulfone trans-heptachlor epoxide tebuconazole boscalid op-ddt fenthion sulfoxide methacrifos tecnazene cis-chlordane pp -DDT fenvalerate methidathion triazophos trans-chlordane deltamethrin fluazifop 4,4 -methoxychlor vinclozolin oxychlordane diazinon fluquinconazole nitrofen PCB 28 chlorfenvinphos dieldrin flusilazole parathion-ethyl PCB 52 chlorobenzilate alpha-endosulfan (endosulfan I) formothion parathion-methyl PCB 101 chlorpropham beta-endosulfan (endosulfan II) hexachlorobenzene (HCB) pendimethalin PCB 118 chlorpyrifos (-ethyl) endosulfan sulfate alpha-hexachlorocyclohexane (-HCH) permethrin (sum isomers) PCB 138 chlorpyrifos-methyl endrin beta-hexachlorocyclohexane (-HCH) pirimiphos-methyl PCB 153 cyfluthrin (sum isomers) epoxiconazole gamma- hexachlorocyclohexane (lindane) profenofos PCB 180 lambda-cyhalothrin famoxadone heptachlor pyrazophos 25 g 25 g 25 g Sayfa 15 / 18

19 Pestisit Kalıntıları Tahıl Ürünleri Her test materyali (0978 hariç) Liste 2'de belirtilen pestisitlerden birkaç tanesini içerir. 11/05/ maize flour selection from list 2 24/07/ wheat flour selection from list b blank wheat flour BLANK (only available if ordered with test 0977) 05/09/ cereal chlormequat (single pesticide) 03/10/ brown rice selection from List 2 22/11/ baby food selection from List 2 06/03/ wheat flour selection from list b blank wheat flour BLANK (only available if ordered with test 0981) Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) Liste 2 acephate deltamethrin fenthion sulfone malathion pyrimethanil azinphos-methyl demeton-s-methyl sulfone fenpropimorph methacrifos quintozene azoxystrobin diazinon fenvalerate(sum of isomers) methomyl spiroxamine bifenthrin dichlorvos fipronil omethoate tebuconazole bromophos-ethyl difenoconazole fludioxonil oxydemeton-methyl (demeton-s-methyl sulfoxide) tebufenozide captan diflubenzuron fluquinconazole paclobutrazole terbufos carbaryl dimethoate flusilazole parathion-ethyl terbufos sulfoxide carbendazim dimoxystrobin flutriafol penconazole terbufos sulfone carbofuran disulfoton formothion pendimethalin tetrachlorvinphos 3-hydroxycarbofuran alpha-endosulfan (endosulfan I) alpha-hexachlorocyclohexane (-HCH) carboxin beta-endosulfan (endosulfan II) beta-hexachlorocyclohexane (-HCH) permethrin (sum) phorate thiabendazole thiacloprid chlorfenvinphos endosulfan sulfate gamma-hch (lindane) phorate sulfoxide thiamethoxam chlorothalonil epoxiconazole hexaconazole phorate sulfone thiodicarb chlorpropham ethion imazalil phosalone triadimefon chlorpyrifos ethoprophos imidacloprid phosmet triadimenol chlorpyrifos-methyl etrimphos iprodione phosphamidon (sum of isomers) triazophos clothianidin fenamiphos isofenphos-methyl pirimicarb tricyclazole cyfluthrin (sum of isomers) fenamiphos sulfoxide isoprothiolane desmethyl-pirimicarb trifloxystrobin lambda-cyhalothrin fenamiphos sulfone isoproturon pirimiphos-methyl trifluralin cypermethrin fenbuconazole kresoxim-methyl prochloraz triticonazole cyproconazole fenhexamid linuron pyraclostrobin vinclozolin cyprodinil fenitrothion malaoxon pyridaphenthion disulfoton sulfoxide fenthion metconazole procymidone disulfoton sulfone fenthion sulfoxide metribuzin propiconazole Sayfa 16 / 18

20 Pestisit Kalıntıları Taze ve kuru meyveler, Taze sebzeler, Çay ve aromatik otlar Meyve, sebze ve aromatic ot matriksleri taze meyve, sebze veya otların püre haline getirilmesiyle hazırlanacaktır. Herbir test materyali (19145 hariç) Liste 3'te belirtilen pestisitlerden birkaçını içerir Liste 4'te belirtilen pestisitlerden birkaçını içerir. 30/04/ P apple pesticide residues from List 3 90 g 19133b P blank apple BLANK 90 g 30/04/ P lemon pesticide residues from List 3 90 g 19134b P blank lemon BLANK 90 g 28/05/ P tomato pesticide residues from List 3 90 g 19135b P blank tomato BLANK 90 g 28/05/ P dried vine fruit pesticide residues from List 3 90 g (raisin) 19136b P blank dried vine fruit BLANK 90 g (raisin) 17/09/ P strawberry pesticide residues from List 3 90 g 19137b P blank strawberry BLANK 90 g 17/09/ P sweet (bell) pepper 19138b P blank sweet (bell) pepper pesticide residues from List 3 BLANK 22/10/ P apricot pesticide residues from List 3 90 g 19139b P blank apricot BLANK 90 g 22/10/ P lettuce pesticide residues from List 3 90 g 19140b P blank lettuce BLANK 90 g 26/11/ P green beans (inc. pods) 19141b P blank green beans (inc. pods) pesticide residues from List 3 BLANK 26/11/ P melon pesticide residues from List 3 90 g 19142b P blank melon BLANK 90 g 14/01/ P basil (herb) pesticide residues from List 3 90 g 19143b P blank basil (herb) BLANK 90 g 14/01/ P cabbage pesticide residues from List 3 90 g 19144b P blank cabbage BLANK 90 g 18/01/ tea pesticide residues from List b blank tea BLANK 18/02/ P grape pesticide residues from List 3 90 g 19146b P blank grape BLANK 90 g 18/02/ P pear pesticide residues from List 3 90 g 19147b P blank pear BLANK 90 g 18/03/ P potato pesticide residues from List 3 90 g 19148b P blank potato BLANK 90 g 18/03/ P orange pesticide residues from List 3 90 g 19149b P blank orange BLANK 90 g 90 g 90 g 90 g 90 g Footnotes BLANK nuumuneler sadece ilgili yeterlik testi ile birlikte sipariş edilebilir P matriks püredir Sayfa 17 / 18

21 Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) Liste 2,4-D cypermethrin (sum of isomers) fenarimol metaflumizone (sum of isomers) prothiofos 2-phenylphenol cyproconazole fenazaquin metalaxyl pymetrozine acephate cyprodinil fenbuconazole metconazole pyraclostrobin acetamiprid pp -DDD (TDE) fenhexamid methamidophos pyrazophos acrinathrin pp -DDE fenitrothion methidathion pyrethrins (sum) aldicarb op -DDT fenoxycarb methiocarb pyridaben aldicarb sulfone pp -DDT fenpropathrin methiocarb sulfone pyrimethanil (aldoxycarb) deltamethrin fenpropimorph methiocarb sulfoxide pyriproxyfen aldicarb sulfoxide demeton-s-methyl sulfone fenpyroximate methomyl quinalphos amitraz desmethyl-pirimicarb fenthion 4,4 -methoxychlor quinoxyfen atrazine diazinon fenthion sulfoxide methoxyfenozide quintozene azinphos-methyl dichlofluanid fenthion sulfone monocrotophos spinosad (spinosyn A + spinosyn D) azoxystrobin dichlorvos fenvalerate myclobutanil spiroxamine (sum of isomers) bifenthrin dicloran fipronil omethoate tebuconazole biphenyl dicofol fipronil sulfone oxadixyl tebufenozide (sum of isomers) bitertanol dicrotophos fluazifop-p-butyl (sum) oxamyl tebufenpyrad boscalid diethofencarb fludioxonil oxydemeton-methyl tecnazene (demeton-s-methyl sulfoxide) bromopropylate diethofencarb sulfoxide flufenoxuron oxyfluorfen teflubenzuron bromuconazole diethofencarb sulfone fluquinconazole paclobutrazol tefluthrin (sum of isomers) bupirimate difenoconazole flusilazole paraoxon-methyl terbufos buprofezin diflubenzuron flutriafol parathion (-ethyl) terbufos sulfoxide butocarboxim dimethoate folpet parathion-methyl terbufos sulfone butocarboxim sulfoxide dimethomorph formetanate HCl penconazole terbuthylazine (sum of isomers) cadusafos diniconazole fosthiazate pencycuron tetraconazole carbaryl diphenylamine haloxyfop (free acid) pendimethalin tetradifon carbendazim DMST HCB (hexachlorobenzene) permethrin thiabendazole (sum of isomers) carbofuran dodine hexaconazole phenthoate thiacloprid 3-hydroxy carbofuran alpha-endosulfan hexythiazox phosalone thiamethoxam chlorfenapyr (endosulfan I) imazalil phosmet thiodicarb chlorfenvinphos beta-endosulfan imidacloprid phoxim tolclofos-methyl (sum of isomers) chlorobenzilate (endosulfan II) indoxacarb pirimicarb tolylfluanid (sum isomers) chlorothalonil endosulfan sulfate iprodione pirimiphos-methyl triadimefon chlorpropham EPN iprovalicarb prochloraz (sum) triadimenol chlorpyrifos (-ethyl) epoxiconazole isofenphos-methyl procymidone triazophos chlorpyrifos-methyl ethion isoprocarb profenofos trifloxystrobin chlorthal-dimethyl ethoprophos isoproturon propamocarb trifluralin chlozolinate etofenprox kresoxim-methyl propaquizafop triticonazole clofentezine famoxadone lenacil propargite vinclozolin clothianidin fenamiphos linuron propiconazole zoxamide cyfluthrin fenamiphos sulfone lufenuron propoxur (sum of isomers) lambda-cyhalothrin fenamiphos sulfoxide mepanipyrim propyzamide Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) Liste 4 bifenthrin dicofol alpha-endosulfan (endosulfan I) fenpropathrin quinalphos chlorothalonil dimethoate beta-endosulfan (endosulfan II) fenvalerate (sum isomers) trifloxystrobin chlorpyrifos (-ethyl) pp -DDD (TDE) endosulfan sulfate HCB (hexachlorobenzene) lambda-cyhalothrin pp -DDE ethion phosalone cypermethrin (sum isomers) op -DDT fenazaquin procymidone deltamethrin pp -DDT fenitrothion propargite Sayfa 18 / 18