1. Lütfen katılmak istediğiniz testleri Program sayfalarında işaretleyiniz. Notlar a) İlginizi çekebilecek testleri daha kolay bulabilmeniz için indeks sayfasını kullanabilirsiniz. b) Belirtilen dağıtım tarihleri planlanan tarihlerdir. Kayıt yaptıdırdığınız testlerden, herhangi bir sebeple ertelenenler olduğu takdirde email ile tarafınıza bildirilecektir. Testlerin büyük bir bölümünün kapanış tarihleri dağıtım tarihlerinden itibaren 6-8 haftadır. c) Her test için test materyallerinin yaklaşık miktarları verilmiştir. Metodunuz daha fazla materyal gerektiriyorsa lütfen ekstra test materyal sayısını bildiriniz. İlave test materyaller için ücret ödenir. d) Ekstra test materyalleri ilave performans değerlendirmesi hakkı kazandırmaz. Birden fazla değerlendirme için çoklu kayıt yaptırmanız gerekmektedir. e) Test materyalleri DHL ile gönderilir. 2. Kayıtlar: FAPAS Programına kayıtlar için Fera Standard Terms and Conditions for Proficiency Testing Schemes dokümanında belirtilen şartlar geçerlidir. Dokümana www.fapas.com adresinden ulaşılabilir. Notlar a) 30 gün içerisinde kayıt onayınız ulaşmazsa lütfen iletişime geçiniz. b) Siparişiniz alındığında faturanız kesilecektir. Bu, ödemelerin testlerden önce yapılacağı anlamına gelmektedir. 3. İlave notlar: i. Dağıtım a) Yukarıda da belirtildiği gibi, numuneler DHL ile gönderilmektedir. Bazı paketler sıcaklık değişimlerini minimize etmek için buz bloklar içerir ancak soğuk araçlarda taşınmamaktadır. Numuneniz elinize ulaştığında sıcaklığı yüksek de olsa, taşıma süresinin büyük bölümünde soğuk kaldığından dolayı testler için uygundur. b) Numuneniz dağıtımdan itibaren 4 gün içerisinde elinize ulaşmadığında lütfen iletişime geçiniz. c) Numuneler gönderildiğinde, kayıtlı olan email adresine FAPAS tarafından DHL takip numarası Airway Bill Number gönderilecektir. d) Takip numaralarına kullanıcı adı ve şifrenizle girdiğiniz FAPAS web sitesindeki sayfanızdan da ulaşabilirsiniz. e) Numunelerin takibi katılımcı sorumluluğundadır. ii. Gümrük a) Test materyallerinin gümrüklerdeki muhtemel hasar ve kayıplarından veya olası gümrük işlemlerinden FAPAS sorumlu değildir. iii. Sonuçlar a) Katılımcıların sonuçları bildirmesi için numune dağıtım tarihinden itibaren genellikle 6 haftaları bulunmaktadır. Bazı analizler test materyali ve/veya analitlerden kaynaklanan nedenlerden dolayı daha kısa sürede tamamlanmalıdır. Bu testler programda belirtilmektedir. b) Sonuçlar FAPAS web sitesi üzerinden kabul edilmektedir. iv. Raporlar a) Test fiyatlarına katılımcıların kullanıcı adı şifreleriyle giriş yaptığı sistemde görebileceği elektronik rapor dahildir. b) Raporlar genellikle testin kapanmasından 5 hafta sonra web sitesinde yayımlanır. c) Raporlar PDF formatında ve dijital imzalı olarak sunulmaktadır. Görüntülemek için Adobe Reader 7 veya üzeri gerekmektedir.
Index 2011 2012 FAPAS YETERLİK TESTLERİ PROGRAMI 3-MCPD & 1,3 DCP...2 acesulfame-k...11 acidity...12 acrylamide...2 aflatoxins...7 ALA...12 alcoholic strength...11 almond...5, 7 almond protein...5 aluminium...10 animal (pork) fat...13 animal feed...7, 8 anisidine value...12 antimony...10 antioxidants...9 apple juice...7, 11 apple purée...7, 15 ARA...12 arsenic...10 arsenic, inorganic...10 ash...1, 5 aspartame...11 avermectins...4 barley flour...8, 14 basmati rice...3 beef...3 benzoic acid...9, 11 beta-agonists...4 beta-lactoglobulin...5 biscuits...2 bisphenol A...6 bovine kidney...4 bovine milk...4 bovine urine...4 brandy...11 bread...6 breadcrumbs...1 breakfast cereal...6, 8, 9 brix...9, 11 butter...1 butyric acid...1, 12 cabbage purée...3 cadmium...10 caffeine...9, 11 cake mix...5 calcium...5, 6, 11 canned fish...5 canned meat...1, 6 canned meat meal...1 casein...5 cereal...1, 7, 8, 12, 14 cheese...1 cheese & pasta meal...1 cherry purée...15 chicken...3 chilli powder...7, 10 chilli sugar paste...10 chloramphenicol...4 chloride...1, 9 chlormequat...14 chocolate...1, 5 chocolate cake mix...9 cholesterol...12 chromium...10 citric acid...9, 11 coccidiostats...4 cocoa...8, 10 cola drink...11 colours...11 condensed milk...1 copper...5, 10 corn/maize...1 corned beef...4 crab meat...10 cranberry juice...11 crispbread...2 crude fibre...5 cyclamate...11 dairy ration...5 deoxynivalenol (DON)...8 DHA...12 diastase...2 dihydrostreptomycin...4 dried apricot...9 dried figs...7 dried vine fruit...8 edible oil...10 egg...5 egg, egg white protein...5 eggs...4 energy drink...6 ethanal (acetaldehyde)...11 ethyl acetate...11 ethyl carbamate...11 fatty acids...12 fish...1, 3, 4, 5, 10, 12 fish identification...3 fish muscle...4 fish oil...12 fish paste...1 fluoroquinolones...4 food simulant...6 fructose...2, 11 fruit juice...10 fruit purée...9 fumonisins...8 ginger (spice)...7 glucose...2, 11 gluten...5 grape purée...15 grapefruit juice...11 green bean purée...15 green coffee...8 ground coffee...11 hazelnut (water/nut slurry)...7 higher alcohols (sum)...11 histamine...5 honey...2, 4 hot pepper sauce...9 hydrogenated vegetable oil...13 hydroxymethylfurfural (HMF)...2 hydroxyproline...1 illegal dyes...9 immersion in ethanol...6 immersion in olive oil...6 infant cereal...10 infant formula...10, 12 infant soya formula...5 instant coffee...8 iodine...6, 12 iodine value...12 iron...5, 6, 10 jam...5, 9 k232 & k270...12 lactose...1 lamb...3 LCPUFAs...12 lead...5, 10 lettuce purée...3, 15 leucomalachite green...4 linoleic acid...12 liquid vitamin supplement...9 magesium...5 magnesium...5, 6, 11 maize...7 maize flour...8, 14 malachite green...4 manganese...5, 6 meat...3, 9 melamine...2, 6 mercury...10 mercury, methyl...10 methanol...11 methylbutanol...11 milk...5 milk powder...1, 2, 3, 6, 7, 9, 10, 13 mixed fat spread...12 mixed fruit drink...15 moisture...1, 2, 5 molybdenum...10 nitrate...3 nitrite...3 nitrofuran metabolites...4 nitrofurans...4 nitrogen...1 non-fat solids...1 non-permitted colours...9 NSAIDs...4 NSP fibre...1 nutritionally fortified oil...12 nylon film...6 oat flour...8 ochratoxin A...8 oil...6, 9
Oils & Fats...12 prawns...4 tea...15 oily fish...13 olive oil...6, 12, 13 omega-3 & omega-6...12 orange juice...11 overall migration...6 PAHs...6 PAHs (EU priority)...6 palm oil...6 paprika...8 patulin...7 peanut...5, 7 peanut, peanut protein...5 pear purée...15 permitted colours...9 peroxide value...12 pesticide residues...13, 14, 15, 16 ph...9, 11 phosphoric acid (as P2O5)...11 phosphorus...5, 6, 11 phthlates...6 pig kidney...4 pig liver...4 pig ration...5 pistachio (water/nut slurry)...7 plastic film...6 polyphosphates...1 pork...3 porridge oats...1 potassium...6, 11 potato purée...15 poultry ration...5 powdered baby food...9 powdered rice...10 premix...5 protein...5 quinine...11 quinolones...4 quinolones & fluoroquinolones...4 refined palm oil...2 rice...3, 7 rice (brown)...14 roasted coffee...8 saccharin...11 saturated FAs...12 selenium...5, 6, 10 sheep feed...5 smoked meat...6 snack food...1 sodium...1, 5, 6, 9, 11 soft drink...10, 11 sorbic acid...9, 11 soy sauce...2 soya flour...10 soya, soya protein...5 spinach purée...3 starch...1, 5 strawberry purée...15 streptomycin...4 sucrose...1, 2, 9, 11 sugar confectionary...9 sulfonamides...4 sulphites...5 sulphur dioxide...9 sweet (bell) pepper purée...15 synthetic hormones...4 T-2 & HT-2 toxins...8 tequila...11 tetracyclines...4 theobromine...9 tin...10 titratable acidity...1 tomato paste...10 tomato purée...15 tomato sauce...9 tonic water...11 total acidity...9, 11 total dietary fibre...1 total fat...1, 12 total folate...9 total niacin...9 total oil...5 total primary aromatic amines...6 total SO2...11 total sugars...1, 5, 9, 11 total volatile basic nitrogen (TVB-N)..1 trans fatty acids...12 unsaturated FAs, mono...12 unsaturated FAs, poly...12 vegetable oil...12 vegetable purée...10 vitamins...5, 9 volatile acidity...11 wheat flour...1, 5, 8, 14 whisky...11 wine...8, 10, 11, 15 zearalenone (ZON)...8 zinc...5, 6, 10 lemon purée...15 β-agonists...4
Besin Bileşenleri 08/04/2011 0173 canned meat moisture, ash, total fat, nitrogen, sodium & chloride 04/05/2011 0174 canned meat meal moisture, ash, total fat, nitrogen, sodium & chloride 01/06/2011 0175 canned meat moisture, ash, total fat, nitrogen, hydroxyproline 26/08/2011 0176 canned meat moisture, ash, total fat, nitrogen, hydroxyproline 01/12/2011 0177 canned meat meal moisture, ash, total fat, nitrogen, sodium, chloride, total sugars 15/02/2012 0178 canned meat moisture, ash, total fat, nitrogen, sodium, chloride & polyphosphates 28/04/2011 2442 wheat flour moisture at 130 C, ash, nitrogen & total dietary fibre by AOAC 08/06/2011 2443 porridge oats moisture at 130 C, ash, total fat, nitrogen, total dietary fibre by AOAC & NSP fibre by Englyst 29/09/2011 2444 cereal moisture at 130 o C, ash, nitrogen & total dietary fibre by AOAC 19/01/2012 2445 breadcrumbs moisture, ash, nitrogen, starch & total dietary fibre by AOAC 25/05/2011 2590 corn/maize snack food moisture, ash, total fat, nitrogen, sodium & chloride 24/06/2011 2591 fish paste moisture, ash, total fat, nitrogen, sodium & chloride 19/08/2011 2592 condensed milk moisture, ash, total fat, nitrogen & total sugars 1 1 1 1 1 1 1 1 1 1 1 150 ml 23/09/2011 2593 canned fish total volatile basic nitrogen (TVB-N) 1 17/10/2011 2594 chocolate moisture, total fat, butyric acid, lactose & sucrose 03/01/2012 2595 milk powder moisture, ash, total fat, nitrogen, titratable acidity & lactose 06/02/2012 2596 butter moisture, total fat, non-fat solids, ph & chloride 07/03/2012 2597 cheese & pasta meal moisture, ash, total fat, nitrogen, sodium & chloride Dipnotlar total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa, fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı. 1 200 g 100 g 1
2011 2012 FAPAS YETERLİK TESTLERİ PROGRAMI Acrylamide / Melamine / 3-MCPD 27/04/2011 3030 crispbread acrylamide 12/08/2011 3031 milk powder melamine & cyanuric acid (low levels, <5 mg/kg) 20/10/2011 3032 biscuits acrylamide 16/02/2012 3033 milk powder melamine and cyanuric acid (> 5mg/kg) 27/05/2011 2630 soy sauce 3-MCPD & 1,3 DCP 40 g 21/09/2011 2631 refined palm oil esters of 3-MCPD 50 ml 08/02/2012 2632 soy sauce 3-MCPD & 1,3 DCP 40 g Honey 14/06/2011 2822 honey moisture, fructose, glucose, sucrose, hydroxymethylfurfural (HMF) & diastase 22/11/2011 2823 honey a moisture, fructose, glucose, sucrose, hydroxymethylfurfural (HMF) & diastase 100 g 100 g Dipnotlar a bu test materyali tağşişli bal olabilir 2
Authenticity 13/04/2011 2940 D chicken contamination (presence/absence) of matrix with one or more from: beef, lamb or pork 25/05/2011 2941 R rice identification of EU approved Basmati rice types and identification and quantification of EU non-approved Basmati rice types 22/07/2011 2942 D lamb contamination (presence/absence) of matrix with one or more from: beef, chicken or pork 27/09/2011 2943 fish identification of unknown fish (3 samples) selected from the following list: Gadus morhua, (Linnaeus 1758) Limanda limanda, (Linnaeus 1758) Melanogrammus aeglefinus, (Linnaeus 1758) Merluccius merluccius, (Linnaeus 1758) Hippoglossus hippoglossus, (Linnaeus 1758) Pleuronectes platessa, (Linnaeus 1758) Pollachius virens, (Linnaeus 1758) Merlangius merlangus, (Linnaeus 1758) 02/12/2011 2944 D beef contamination (presence/absence) of matrix with one or more from: chicken, lamb or pork 30 g 2 x 10 g 30 g 3 x 10 g 30 g Nitrate & Nitrite 26/04/2011 1573 cabbage purée nitrate 70 g 30/06/2011 1574 φ meat nitrate & nitrite 25 g 15/08/2011 1575 lettuce purée nitrate 70 g 19/10/2011 1576 φ milk powder nitrate & nitrite (low level) 40 g 30/11/2011 1577 φ meat nitrate & nitrite 25 g 24/01/2012 1578 spinach purée nitrate 70 g 28/03/2012 1579 φ meat nitrate & nitrite 25 g Dipnotlar R test Basmati Rice numunelerinin AB düzenlemelerine uygunluğunun/uygunsuzluğunun tespitine yöneliktir D dondurarak kurutulmuş (freeze dried) numune, analizden önce tekrar sulandırılmalıdır. φ testin süresi kısadır 3
Veteriner İlaç Kalıntıları 12/04/2011 02168 honey streptomycin & dihydrostreptomycin 20 g 03/05/2011 02169 φ prawns chloramphenicol 20 g 17/05/2011 02170 φ# fish muscle tetracyclines 20 g 21/06/2011 02171 φ# prawns nitrofuran metabolites 20 g 05/07/2011 02172 φ fish muscle malachite green, leucomalachite green, total malachite green 20 g 08/08/2011 02173 φ# pig kidney sulfonamides 20 g 22/08/2011 02174 φ# fish muscle quinolones & fluoroquinolones 20 g 20/09/2011 02175 φ# corned beef avermectins 20 g 04/10/2011 02176 φ# pig liver β-agonists 20 g 25/10/2011 02177 honey chloramphenicol 20 g 01/11/2011 02178 φ# bovine kidney tetracyclines 20 g 29/11/2011 02179 φ# chicken eggs nitrofuran metabolites 20 g 13/12/2011 02180 φ fish muscle (oily fish) malachite green leucomalachite green, total malachite green 17/01/2012 02181 # honey sulfonamides 20 g 07/02/2012 02182 # bovine milk (milk powder) 28/02/2012 02183 # chicken egg (whole egg powder) NSAIDs (nonsteroidal anti-inflammatory drugs) coccidiostats 20/03/2012 02184 φ# bovine urine synthetic hormones 25 ml Testlerde belirtilen genel kategorilerdeki muhtemel ilaç kalıntılarının listesi - Liste A. tetracyclines chlortetracycline (total), doxycycline, oxytetracycline (total), tetracycline (total) nitrofurans AHD (bound), AHD (total), AOZ (bound), AOZ (total), AMOZ (bound), AMOZ (total), SEM (bound), SEM (total) sulfonamides sulfachloropyridazine, sulfadiazine, sulfadimethoxine, sulfadimidine (sulfamethazine), sulfadoxine, sulfaguanadine, sulfamerazine, sulfamethizole, sulfamethoxazole, sulfamethoxypyridazine, sulfamonomethoxine, sulfamoxole, sulphanilamide, sulfapyridine, sulfaquinoxaline, sulfathiazole, sulfisoxazole quinolones & fluoroquinolones flumequine, nalidixic acid, oxolinic acid, ciprofloxacin, danofloxacin, difloxacin, enrofloxacin, marbofloxacin, norfloxacin, sarafloxacin avermectins abamectin, doramectin, emamectin, eprinomectin, ivermectin, moxidectin β-agonists bromobuterol, cimaterol, cimbuterol, clenbuterol, clenpenterol, hydroxyclenbuterol, mabuterol, mapenterol, ractopamine, salbutamol, salmeterol, terbutaline, tulobuterol, zilpaterol synthetic hormones α-boldenone, methylboldenone, diethylstilbestrol (DES), dienestrol, hexoestrol, methyltestosterone, α-nortestosterone, stanozolol, 16β-hydroxystanozolol, trenbolone, zeranol nonsteroidal anti-inflammatory drugs diclofenac, 5-hydroxyflunixin, ibuprofen, meloxicam, naproxen, phenylbutazone (NSAIDs) ) coccidiostats diclazuril, lasalocid, maduramycin, monensin, narasin, nicarbazin (as 4,4-dinitrocarbanilide), salinomycin Dipnotlar # test Liste A'da belirtilen analitlerin belirlenmesi ve miktar tayinlerini içerir. φ testin süresi kısadır. 20 g 20 g 20 g 4
Yem Maddeleri 19/05/2011 1093 dairy ration moisture, ash, total oil, protein & crude fibre 1 19/05/2011 1094 dairy ration iron, lead, magnesium, manganese & selenium 1 16/06/2011 1095 sheep feed moisture, ash, total oil, protein & copper 1 06/10/2011 1096 pig ration moisture, ash, total oil, protein, crude fibre, vitamin E & zinc 1 24/11/2011 1097 poultry ration moisture, ash, total oil, protein & crude fibre 1 24/11/2011 1098 poultry ration starch, total sugars, calcium & phosphorus 1 09/02/2012 1099 premix calcium, manganese, magnesium, phosphorus, sodium & zinc 1 09/02/2012 10100 premix vitamin A, D 3, E 1 Allerjenler Histamin ve sülfitler DIŞINDA (genellikle HPLC metotları kullanılır), sonuçlar ELISA kitlerinin markasına göre gruplandırılarak değerlendirilir. 13/04/2011 2789 infant soya formula casein 2 x 20 g 04/05/2011 2790 canned fish histamine (high level) 145 g 08/06/2011 2791 cake mix egg, egg white protein 2 x 20 g 30/06/2011 2792 infant soya formula gluten 2 x 20 g 21/07/2011 2793 chocolate peanut, peanut protein 2 x 20 g 04/08/2011 2794 infant soya formula beta-lactoglobulin 2 x 20 g 24/08/2011 2795 cake mix gluten 2 x 20 g 01/09/2011 2796 canned fish histamine (low level) 145 g 21/09/2011 2797 chocolate hazelnut, hazelnut protein 2 x 20 g 18/10/2011 2798 jam sulphites 20 g 02/11/2011 2799 cake mix gluten, milk and egg 30 g 04/01/2012 27100 wheat flour soya, soya protein 2 x 20 g 17/02/2012 27101 canned fish histamine (high level) 145 g 01/03/2012 27102 chocolate almond, almond protein 2 x 20 g Dipnotlar total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa, fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı. iki adet test materyali gönderilir. Kalitatif ve kantitatif sonuçlar bildirilebilir. Kalitatif ve kantitatif sonuçlar bildirilebilir. 5
Çevresel Bulaşanlar 20/04/2011 0648 palm oil PAHs 30 ml 20/09/2011 0649 smoked meat product PAHs 05/01/2012 0650 olive oil all 16 EU priority PAHs 30 ml Migrasyon Overall & Specific 20/04/2011 1142 nylon film overall migration into ethanol by total immersion 03/11/2011 1143 plastic film overall migration into olive oil by total immersion 40 cm x 22 cm 40 cm x 22 cm 29/06/2011 1245 B food simulant phthalates 2 x 50 ml 17/08/2011 1246 3% w/v acetic acid in water melamine 1 x 50 ml 07/09/2011 1247 B food simulant bisphenol A 2 x 50 ml 17/11/2011 1248 food simulant total primary aromatic amines >300 ml 08/03/2012 1249 oil photo initiators >50 ml Besin Elementleri 07/04/2011 1862 canned meat calcium, phosphorus & zinc (all natural levels) 1 14/07/2011 1863 breakfast cereal calcium, iron & zinc (fortified) 10/08/2011 1864 bread sodium 16/11/2011 1865 milk powder calcium, iodine & selenium, (all natural levels) 23/03/2012 1866 energy drink iron, magnesium, manganese, potassium, selenium, (all natural levels) Dipnotlar B Blank matriks dahildir. 6
Mikotoksinler Aflatoxins 04176 ve 04181 ELISA taramaları yapan laboratuvarlara yöneliktir. 19/04/2011 04173 pistachio (water/nut slurry) aflatoxins B & G &/or total 100 g 27/04/2011 04174 maize aflatoxins B & G &/or total 55 g 12/05/2011 04175 milk powder aflatoxin M 1 55 g 16/06/2011 04176 maize aflatoxin B 1, DON, ZON & OTA 1 06/07/2011 04177 chilli powder aflatoxins B & G &/or total 55 g 28/07/2011 04178 animal feed (cereal based) aflatoxins B & G &/or total 55 g 31/08/2011 04179 maize aflatoxins B & G &/or total 55 g 08/09/2011 04180 milk powder aflatoxin M 1 55 g 15/09/2011 04181 maize aflatoxin B 1, DON, ZON & OTA 1 26/09/2011 04182 hazelnut (water/nut slurry) 10/10/2011 04183 almond (water/nut slurry) aflatoxins B & G &/or total aflatoxins B & G &/or total 100 g 100 g 02/11/2011 04184 peanut aflatoxins B & G &/or total 55 g 23/11/2011 04185 ginger (spice) aflatoxins B & G &/or total 55 g 06/01/2012 04186 animal feed (cereal based) 31/01/2012 04187 pistachio (water/nut slurry) aflatoxins B & G &/or total aflatoxins B & G &/or total 55 g 100 g 08/02/2012 04188 rice aflatoxins B & G &/or total 55 g 29/02/2012 04189 peanut aflatoxins B & G &/or total 55 g 12/03/2012 04190 dried figs (water/fruit slurry) aflatoxins B & G &/or total 100 g 22/03/2012 04191 milk powder aflatoxin M 1 55 g Mikotoksinler Patulin 13/06/2011 1644 apple juice (clear) patulin 50 ml 11/10/2011 1645 apple purée patulin 60 g 27/03/2012 1646 apple juice (cloudy) patulin 50 ml 7
Mikotoksinler Okratoksin A 05/05/2011 17100 maize flour ochratoxin A 55 g 20/06/2011 17101 dried vine fruit (water/fruit slurry) ochratoxin A 100 g 08/07/2011 17102 barley flour ochratoxin A 55 g 11/08/2011 17103 green coffee ochratoxin A 55 g 09/09/2011 17104 paprika ochratoxin A 55 g 27/10/2011 17105 instant coffee ochratoxin A 55 g 07/12/2011 17106 wine ochratoxin A 55 ml 10/01/2012 17107 wheat flour ochratoxin A 55 g 02/02/2012 17108 roasted coffee ochratoxin A 55 g 02/03/2012 17109 animal feed ochratoxin A 55 g 29/03/2012 17110 cocoa ochratoxin A 55 g Mikotoksinler Fusarium toksinleri 07/04/2011 2274 maize flour deoxynivalenol (DON) 55 g 12/05/2011 2275 maize flour FB 1 & FB 2 (not total fumonisins) 55 g 13/07/2011 2276 animal feed zearalenone (ZON) 55 g 02/08/2011 2277 animal feed deoxynivalenol (DON) 55 g 30/08/2011 2278 breakfast cereal zearalenone (ZON) 55 g 26/10/2011 2279 breakfast cereal deoxynivalenol (DON) 55 g 12/01/2012 2280 oat flour T-2 & HT-2 toxins 55 g 10/02/2012 2281 wheat flour deoxynivalenol (DON) 55 g 15/03/2012 2282 animal feed T-2 & HT-2 toxins 55 g 8
Vitaminler 26/05/2011 2171 φ fruit purée vitamin C 100 ml 15/07/2011 2172 breakfast cereal vitamins B 1, B 2 (total) & B 6, total niacin & total folate 15/11/2011 2173 liquid vitamin supplement vitamins B 1, B 2 (total) & B 6 40 ml 25/01/2012 2174 milk powder vitamins A & D 3 14/03/2012 2175 powdered baby food Gıda Katkı Maddeleri vitamins A, B 12, C & E 06/04/2011 2083 tomato sauce brix, ph, total acidity, sodium & chloride 1 10/05/2011 2084 meat sulphur dioxide 100 g 22/06/2011 2085 jam brix, ph, benzoic acid, citric acid & sorbic acid 16/08/2011 2086 chocolate cake mix 13/09/2011 2087 dried apricot (water/fruit slurry) 19/10/2011 2088 sugar confectionary (boiled sweets) caffeine, sorbic acid, theobromine & total sugars (expressed as sucrose) sulphur dioxide permitted colours up to 4 selected from the following list: Allura Red, Brilliant Blue FCF, Carmoisine, Erythrosine, Green S, Indigo Carmine, Patent Blue V, Ponceau 4R, Quinoline Yellow, Sunset Yellow FCF, Tartrazine 08/12/2011 2089 oil antioxidants: total BHA (E320), BHT (E321) & propyl gallate (E310) 01/02/2012 2090 hot pepper sauce (or similar) non-permitted colours (illegal dyes) up to 4 selected from the following list: Butter Yellow (Dimethyl Yellow), Orange II, Para Red, Rhodamine B, Sudan I, Sudan II, Sudan III, Sudan IV, Sudan Black B, Sudan Orange G, Sudan Red B, Sudan Red 7B, Sudan Red G, Toluidine Red 100 g 50 ml 50 ml Dipnotlar total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa, fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı. φ testin süresi kısadır. Kalitatif ve kantitatif sonuçlar bildirilebilir. 9
Metalik Bulaşanlar 14/04/2011 07154 milk powder arsenic, cadmium, (natural levels), mercury, lead, (high levels) 11/05/2011 07155 soft drink antimony, arsenic (total) cadmium, chromium copper & zinc (all high levels) 15/06/2011 07156 canned fish arsenic (total), lead, cadmium & mercury (total) (all natural levels) 50 ml 1 28/06/2011 07157 tomato paste cadmium, lead, iron & tin (all high levels) 20/07/2011 07158 chilli powder arsenic (total), cadmium & lead (all high levels) 03/08/2011 07159 infant formula aluminium, chromium, molybdenum, selenium (all low levels) 25/08/2011 07160 canned crab meat arsenic (total), arsenic (inorganic), cadmium, lead & mercury (total), (all natural levels) 1 14/09/2011 07161 chilli sugar paste lead 25 g 28/09/2011 07162 edible oil arsenic (total), copper, iron & lead (all high levels) 50 ml 05/10/2011 07163 wine ph, cadmium & lead 100 ml 26/10/2011 07164 canned fish arsenic (total), cadmium, mercury (total) (all natural levels) 10/11/2011 07165 infant cereal cadmium, chromium, lead, mercury (total), selenium (all natural levels) 01/12/2011 07166 soya flour aluminium, arsenic (total), cadmium, lead & mercury (total) (all high levels) 13/01/2012 07167 cocoa powder cadmium & lead (both natural levels) 1 14/02/2012 07168 fruit juice cadmium, iron, lead, & tin (all high levels) 50 ml 24/02/2012 07169 powdered rice arsenic (inorganic), arsenic (total) & cadmium (all high levels) 13/03/2012 07170 vegetable purée cadmium, lead & tin (all high levels) 21/03/2012 07171 canned fish arsenic (total), methyl mercury & mercury (total) (all natural levels) 1 10
Meyve Suyu, Alkollü ve Alkolsüz İçecekler 09/06/2011 0840 apple juice brix, ph, total acidity, total sugars, magnesium, potassium & sodium 14/10/2011 0841 orange juice brix, ph, citric acid, sucrose, glucose, fructose & total sugars 26/01/2012 0842 grapefruit juice brix, ph, total acidity, total sugars, calcium, magnesium & potassium 16/03/2012 0843 cranberry juice brix, ph, total acidity, total sugars, phosphorus & potassium 13/05/2011 0397 cola drink benzoic acid, caffeine, acesulfame-k & saccharin 14/07/2011 0398 ground coffee caffeine (2 test materials supplied, one regular, one decaffeinated) 23/08/2011 0399 soft drink brix, ph, citric acid, sorbic acid, cyclamate & saccharin 13/10/2011 03100 soft drink up to 4 colours from the following list: Allura Red, Brilliant Blue FCF, Carmoisine, Erythrosine, Green S, Indigo Carmine, Patent Blue V, Ponceau 4R, Quinoline Yellow, Sunset Yellow FCF, Tartrazine 09/12/2011 03101 cola drink caffeine, benzoic acid, total sugars & phosphoric acid (as P 2O 5) 18/01/2012 03102 tonic water benzoic acid, quinine, acesulfame-k & aspartame 18/05/2011 1361 whisky alcoholic strength, ethanal (acetaldehyde), ethyl acetate, methanol, propan-1-ol, 2-methylpropanol & 2-methylbutanol + 3-methylbutanol (sum) 08/09/2011 1362 brandy alcoholic strength, ethanal (acetaldehyde), ethyl acetate, methanol, propan-1-ol, 2-methylpropanol & 2-methylbutanol + 3-methylbutanol (sum) & ethyl carbamate 16/11/2011 1363 wine alcoholic strength, total SO 2, total acidity & volatile acidity 22/02/2012 1364 tequila alcoholic strength, ethanal (acetaldehyde), ethyl acetate, methanol, propan-1-ol, 2-methylpropanol & 2-methylbutanol + 3-methylbutanol (sum) 250 ml 250 ml 250 ml 250 ml 150 ml 2 x 30 g 150 ml 150 ml 150 ml 150 ml 200 ml 200 ml 220 ml 200 ml Dipnotlar total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa, fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı. Kalitatif ve kantitatif sonuçlar bildirilebilir. 11
Yağlar 2011 2012 FAPAS YETERLİK TESTLERİ PROGRAMI 26/04/2011 14100 nutritionally fortified oil (may contain LC-PUFAs) 10/05/2011 14101 infant formula (may contain LC-PUFAs) saturates, mono-unsaturates, poly-unsaturates, total trans fatty acids, linoleic acid, α-linolenic acid (ALA), ARA & DHA total fat, saturates, mono-unsaturates, poly-unsaturates, total trans fatty acids, linoleic acid, α-linolenic acid (ALA), ARA, & DHA 07/06/2011 14102 φ olive oil peroxide value, acidity, anisidine value & iodine value 12/07/2011 14103 cereal product (may contain LC-PUFAs) 19/07/2011 14104 nutritionally fortified oil (may contain LC-PUFAs) total fat, saturates, mono-unsaturates, poly-unsaturates, total trans fatty acids, linoleic acid, α-linolenic acid (ALA), ARA, & DHA saturates, mono-unsaturates, poly-unsaturates, total trans fatty acids, linoleic acid, α-linolenic acid (ALA), ARA & DHA 15/08/2011 14105 mixed fat spread total fat, saturates, mono-unsaturates, poly-unsaturates, & trans fatty acids 05/10/2011 14106 φ olive oil peroxide value, acidity, anisidine value & iodine value 30 ml 100 ml 30 ml 100 ml 20/10/2011 14107 fish oil omega-3 & omega-6 series fatty acids 30 ml 08/11/2011 14108 mixed fat spread total fat, butyric acid & cholesterol 19/01/2012 14109 vegetable oil saturates, mono-unsaturates, poly-unsaturates 30 ml 06/03/2012 14110 φ olive oil peroxide value, acidity, K 232 & K 270 100 ml Dipnotlar φ testin süresi kısadır. 12
Pestisit Kalıntıları Hayvansal Ürünler / Yağlar Her hest materyali Liste 1'de belirtilen pestisitlerden birkaç tanesini içerir. 21/04/2011 0576 hydrogenated vegetable oil selection from List 1 25 g 0576b blank hydrogenated vegetable oil BLANK (only available if ordered with test 0576) 25 g 26/05/2011 0577 milk powder selection from List 1 26/07/2011 0578 olive oil selection from List 1 15/09/2011 0579 hydrogenated vegetable oil selection from List 1 25 g 0579b blank hydrogenated vegetable oil BLANK (only available if ordered with test 0579) 25 g 14/11/2011 0580 oily fish selection from List 1 21/02/2012 0581 animal (pork) fat selection from List 1 Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) Liste 1 aldrin lambda-cyhalothrin fenthion methacrifos tecnazene azinphos-ethyl pp -DDE fenthion sulfone methidathion triazophos bifenthrin pp -DDD (TDE) fenthion sulfoxide 4,4 -methoxychlor vinclozolin cis-chlordane op -DDT fenvalerate nitrofen PCB 28 trans-chlordane pp -DDT formothion parathion-ethyl PCB 52 oxychlordane deltamethrin hexachlorobenzene (HCB) parathion-methyl PCB 101 chlorobenzilate diazinon alpha-hexachlorocyclohexane (α-hch) pendimethalin PCB 118 chlorfenvinphos dieldrin beta-hexachlorocyclohexane (β-hch) permethrin (sum isomers) PCB 138 chlorpyrifos (-ethyl) alpha-endosulfan (endosulfan I) gamma- hexachlorocyclohexane (lindane) pirimiphos-methyl PCB 153 chlorpyrifos-methyl beta-endosulfan (endosulfan II) heptachlor profenofos PCB 180 cyfluthrin (sum isomers) endosulfan sulfate cis-heptachlor epoxide pyrazophos cypermethrin endrin trans-heptachlor epoxide quintozene 13
Pestisit Kalıntıları Tahıl Ürünleri Her test materyali (0973 hariç) Liste 2'de belirtilen pestisitlerden birkaç tanesini içerir. 11/05/2011 0971 maize flour selection from list 2 27/07/2011 0972 wheat flour selection from list 2 0972b blank wheat flour BLANK (only available if ordered with test 0972) 12/10/2011 0973 cereal chlormequat (single pesticide) 09/11/2011 0974 brown rice selection from List 2 23/02/2012 0975 barley flour selection from list 2 Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) Liste 2 acephate deltamethrin fenvalerate (sum isomers) metconazole quinoxyfen azinphos-methyl demeton-s-methyl sulfone fipronil methacrifos quintozene azoxystrobin diazinon fludioxonil methomyl spiroxamine bifenthrin dichlorvos fluquinconazole metribuzin tebuconazole captan difenoconazole flusilazole omethoate tebufenozide carbaryl diflubenzuron flutriafol oxydemeton-methyl (demeton-s-methyl sulfoxide) thiabendazole carbendazim (sum of carbendazim, benomyl and thiophanatemethyl ) dimethoate formothion paclobutrazole thiacloprid carbofuran dimoxystrobin alpha-hexachlorocyclohexane (α-hch) 3-hydroxycarbofuran alpha-endosulfan (endosulfan I) beta-hexachlorocyclohexane (β-hch) parathion-ethyl penconazole thiamethoxam thiodicarb carboxin beta-endosulfan (endosulfan II) gamma-hch (lindane) pendimethalin triadimefon chlorfenvinphos endosulfan sulfate hexaconazole permethrin (sum) triadimenol chlorothalonil epoxiconazole imazalil phosmet triazophos chlorpropham ethion imidacloprid phosphamidon (sum isomers) tricyclazole chlorpyrifos etrimphos iprodione pirimicarb trifloxystrobin chlorpyrifos-methyl fenbuconazole isofenphos-methyl desmethyl-pirimicarb trifluralin clothianidin fenhexamid isoprothiolane pirimiphos-methyl triticonazole cyfluthrin (sum) fenitrothion isoproturon prochloraz vinclozolin cypermethrin fenpropimorph kresoxim-methyl procymidone cyproconazole fenthion linuron propiconazole cyprodinil fenthion sulfone malaoxon pyraclostrobin lambda-cyhalothrin fenthion sulfoxide malathion pyrimethanil 14
Pestisit Kalıntıları Taze Meyve ve Sebzeler & İçecekeler Meyve ve sebze matriksleri taze meyve ve sebzelerin püre haline getirilmesiyle hazırlanacaktır. Herbir test materyali (19129 hariç) Liste 3'te belirtilen pestisitlerden birkaçını içerir. 19129 Liste 4'te belirtilen pestisitlerden birkaçını içerir. 14/04/2011 19119 wine pesticide residues from List 3 19119b blank wine BLANK (only available if ordered with test 19119) 18/04/2011 19120 P apple pesticide residues from List 3 19120b P blank apple BLANK (only available if ordered with test 19120) 23/05/2011 19121 P lemon pesticide residues from List 3 90 ml 19121b P blank lemon BLANK 90 ml (only available if ordered with test 19121) 23/05/2011 19122 mixed fruit drink (pasteurised) pesticide residues from List 3 19122b blank mixed fruit drink BLANK (only available if ordered with test 19122) 19/09/2011 19123 P tomato pesticide residues from List 3 90 ml 19123b P blank tomato BLANK 90 ml (only available if ordered with test 19123) 19/09/2011 19124 P strawberry pesticide residues from List 3 19124b P blank strawberry BLANK (only available if ordered with test 19124) 24/10/2011 19125 P sweet (bell) pepper pesticide residues from List 3 19125b P blank sweet (bell) pepper BLANK (only available if ordered with test 19125) 24/10/2011 19126 P cherry pesticide residues from List 3 19126b P blank cherry BLANK (only available if ordered with test 19126) 21/11/2011 19127 P lettuce pesticide residues from List 3 19127b P blank lettuce BLANK (only available if ordered with test 19127) 21/11/2011 19128 P yard long bean (green bean with pods) pesticide residues from List 3 19128 P blank yard long bean (green bean with pods) BLANK (only available if ordered with test 19128) 11/01/2012 19129 tea pesticide residues from List 4 19129b blank tea BLANK (only available if ordered with test 19129) 23/01/2012 19130 P pear pesticide residues from List 3 19130b P blank pear BLANK (only available if ordered with test 19130) 27/02/2012 19131 P grape pesticide residues from List 3 19131b P blank grape BLANK (only available if ordered with test 19131) 27/02/2012 19132 P potato pesticide residues from List 3 19132b P blank potato BLANK (only available if ordered with test 19132) Dipnotlar P matriks püredir 15
Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) Liste 3 2-phenylphenol cyfluthrin (sum isomers) fenbuconazole methiocarb sulfone pyraclostrobin acephate lambda-cyhalothrin fenhexamid methiocarb sulfoxide pyrazophos acetamiprid cypermethrin (sum isomers) fenitrothion methomyl pyrethrins (sum) acrinathrin cyproconazole fenoxycarb 4,4 -methoxychlor pyridaben aldicarb cyprodinil fenpropathrin methoxyfenozide pyrimethanil aldicarb sulfone pp -DDD (TDE) fenpropimorph monocrotophos pyriproxyfen aldicarb sulfoxide pp -DDE fenvalerate (sum isomers) myclobutanil quinalphos amitraz op -DDT fipronil omethoate quinoxyfen atrazine pp -DDT fluazifop-p-butyl oxadixyl spinosad (spinosyn A + spinosyn D) azinphos-methyl deltamethrin fludioxonil oxamyl spiroxamine azoxystrobin demeton-s-methyl sulfone flufenoxuron oxydemeton-methyl tebuconazole (demeton-s-methyl sulfoxide) bifenthrin diazinon fluquinconazole oxyfluorfen tebufenozide bitertanol dichlofluanid flusilazole paclobutrazol tebufenpyrad boscalid dichlorvos flutriafol paraoxon-methyl tecnazene bromopropylate dicloran folpet parathion (-ethyl) teflubenzuron bromuconazole (sum) dicofol formetanate HCl parathion-methyl tefluthrin bupirimate dicrotophos fosthiazate penconazole tetraconazole buprofezin difenoconazole hexaconazole pencycuron tetradifon cadusafos dimethoate hexythiazox pendimethalin thiabendazole carbaryl dimethomorph (sum) imazalil permethrin (sum isomers) thiacloprid carbendazim (sum of diniconazole imidacloprid phenthoate thiamethoxam carbendazim, benomyl & thiophanate-methyl) carbofuran diphenylamine indoxacarb (sum isomers) phosalone thiodicarb 3-hydroxy carbofuran DMST iprodione phosmet tolclofos-methyl chlorfenapyr alpha-endosulfan (endosulfan I) iprovalicarb phoxim tolylfluanid chlorfenvinphos (sum beta-endosulfan (endosulfan II) kresoxim-methyl pirimicarb triadimefon isomers) chlormequat endosulfan sulfate lenacil desmethyl-pirimicarb triazophos (pear and grapes only) chlorobenzilate epoxyconazole linuron pirimiphos-methyl trifloxystrobin chlorthal-dimethyl ethion lufenuron prochloraz trifluralin chlorothalonil ethoprophos mepanipyrim procymidone triticonazole chlorpropham etofenprox metaflumizone profenofos vinclozolin chlorpyrifos (-ethyl) fenamiphos metalaxyl propamocarb zoxamide chlorpyrifos-methyl fenamiphos sulfone metconazole propargite chlozolinate fenamiphos sulfoxide methamidophos propiconazole clofentezine fenarimol methidathion propyzamide clothianidin fenazaquin methiocarb prothiofos Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) Liste 4 bifenthrin dicofol pp -DDT fenazaquin phosalone chlorothalonil dimethoate alpha-endosulfan (endosulfan I) fenitrothion procymidone chlorpyrifos (-ethyl) pp -DDD (TDE) beta-endosulfan (endosulfan II) fenpropathrin propargite lambda-cyhalothrin pp -DDE endosulfan sulfate fenvalerate (sum isomers) quinalphos cypermethrin (sum isomers) op -DDT ethion HCB (hexachlorobenzene) trifloxystrobin deltamethrin 16
İptal Şartları Testin dağıtım tarihine bir aydan daha kısa süre kaldığında iptali istenirse geri ödeme yapılmaz. Dağıtıma bir aydan daha fazla süre varsa test ücretinin %50'si iade edilir veya başka bir testle değiştirilebilir. Faturalandırma & Ödemeler Siparişleriniz bize ulaştığında yeterlik testlerine kayıt bedeli olarak tarafımızdan hizmet faturası düzenlenir. Numunelerin dağıtıımı belirtilen tarihlerde Food and Environment Research Agency tarafından yapılacağından, Sincer Dış Ticaret tarafından bir ürün teslimatı söz konusu değildir. Yeterlik testleri için numuneler belirtilen tarihlerde FERA tarafından DHL ile doğrudan tarafınıza gönderilecektir. Zaman zaman gümrük kontrolleri nedeni ile numunelerin gümrüklerde işlem görmesi olasıdır. Bu durumda numuneler ile ilgili gümrük işlemlerinin tarafınızca yürütülmesi gerekeceğini tekrar hatırlatırız. Ziya Gökalp Bul. 17/4 Alsancak, İzmir 35220 Tel: +90.232.464-8006 Faks: +90.232.464-8007 fapas@sincer.com.tr