FAPAS YETERLİK TESTLERİ PROGRAMI Nisan 2011 Mart 2012

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1 1. Lütfen katılmak istediğiniz testleri Program sayfalarında işaretleyiniz. Notlar a) İlginizi çekebilecek testleri daha kolay bulabilmeniz için indeks sayfasını kullanabilirsiniz. b) Belirtilen dağıtım tarihleri planlanan tarihlerdir. Kayıt yaptıdırdığınız testlerden, herhangi bir sebeple ertelenenler olduğu takdirde ile tarafınıza bildirilecektir. Testlerin büyük bir bölümünün kapanış tarihleri dağıtım tarihlerinden itibaren 6-8 haftadır. c) Her test için test materyallerinin yaklaşık miktarları verilmiştir. Metodunuz daha fazla materyal gerektiriyorsa lütfen ekstra test materyal sayısını bildiriniz. İlave test materyaller için ücret ödenir. d) Ekstra test materyalleri ilave performans değerlendirmesi hakkı kazandırmaz. Birden fazla değerlendirme için çoklu kayıt yaptırmanız gerekmektedir. e) Test materyalleri DHL ile gönderilir. 2. Kayıtlar: FAPAS Programına kayıtlar için Fera Standard Terms and Conditions for Proficiency Testing Schemes dokümanında belirtilen şartlar geçerlidir. Dokümana adresinden ulaşılabilir. Notlar a) 30 gün içerisinde kayıt onayınız ulaşmazsa lütfen iletişime geçiniz. b) Siparişiniz alındığında faturanız kesilecektir. Bu, ödemelerin testlerden önce yapılacağı anlamına gelmektedir. 3. İlave notlar: i. Dağıtım a) Yukarıda da belirtildiği gibi, numuneler DHL ile gönderilmektedir. Bazı paketler sıcaklık değişimlerini minimize etmek için buz bloklar içerir ancak soğuk araçlarda taşınmamaktadır. Numuneniz elinize ulaştığında sıcaklığı yüksek de olsa, taşıma süresinin büyük bölümünde soğuk kaldığından dolayı testler için uygundur. b) Numuneniz dağıtımdan itibaren 4 gün içerisinde elinize ulaşmadığında lütfen iletişime geçiniz. c) Numuneler gönderildiğinde, kayıtlı olan adresine FAPAS tarafından DHL takip numarası Airway Bill Number gönderilecektir. d) Takip numaralarına kullanıcı adı ve şifrenizle girdiğiniz FAPAS web sitesindeki sayfanızdan da ulaşabilirsiniz. e) Numunelerin takibi katılımcı sorumluluğundadır. ii. Gümrük a) Test materyallerinin gümrüklerdeki muhtemel hasar ve kayıplarından veya olası gümrük işlemlerinden FAPAS sorumlu değildir. iii. Sonuçlar a) Katılımcıların sonuçları bildirmesi için numune dağıtım tarihinden itibaren genellikle 6 haftaları bulunmaktadır. Bazı analizler test materyali ve/veya analitlerden kaynaklanan nedenlerden dolayı daha kısa sürede tamamlanmalıdır. Bu testler programda belirtilmektedir. b) Sonuçlar FAPAS web sitesi üzerinden kabul edilmektedir. iv. Raporlar a) Test fiyatlarına katılımcıların kullanıcı adı şifreleriyle giriş yaptığı sistemde görebileceği elektronik rapor dahildir. b) Raporlar genellikle testin kapanmasından 5 hafta sonra web sitesinde yayımlanır. c) Raporlar PDF formatında ve dijital imzalı olarak sunulmaktadır. Görüntülemek için Adobe Reader 7 veya üzeri gerekmektedir.

2 Index FAPAS YETERLİK TESTLERİ PROGRAMI 3-MCPD & 1,3 DCP...2 acesulfame-k...11 acidity...12 acrylamide...2 aflatoxins...7 ALA...12 alcoholic strength...11 almond...5, 7 almond protein...5 aluminium...10 animal (pork) fat...13 animal feed...7, 8 anisidine value...12 antimony...10 antioxidants...9 apple juice...7, 11 apple purée...7, 15 ARA...12 arsenic...10 arsenic, inorganic...10 ash...1, 5 aspartame...11 avermectins...4 barley flour...8, 14 basmati rice...3 beef...3 benzoic acid...9, 11 beta-agonists...4 beta-lactoglobulin...5 biscuits...2 bisphenol A...6 bovine kidney...4 bovine milk...4 bovine urine...4 brandy...11 bread...6 breadcrumbs...1 breakfast cereal...6, 8, 9 brix...9, 11 butter...1 butyric acid...1, 12 cabbage purée...3 cadmium...10 caffeine...9, 11 cake mix...5 calcium...5, 6, 11 canned fish...5 canned meat...1, 6 canned meat meal...1 casein...5 cereal...1, 7, 8, 12, 14 cheese...1 cheese & pasta meal...1 cherry purée...15 chicken...3 chilli powder...7, 10 chilli sugar paste...10 chloramphenicol...4 chloride...1, 9 chlormequat...14 chocolate...1, 5 chocolate cake mix...9 cholesterol...12 chromium...10 citric acid...9, 11 coccidiostats...4 cocoa...8, 10 cola drink...11 colours...11 condensed milk...1 copper...5, 10 corn/maize...1 corned beef...4 crab meat...10 cranberry juice...11 crispbread...2 crude fibre...5 cyclamate...11 dairy ration...5 deoxynivalenol (DON)...8 DHA...12 diastase...2 dihydrostreptomycin...4 dried apricot...9 dried figs...7 dried vine fruit...8 edible oil...10 egg...5 egg, egg white protein...5 eggs...4 energy drink...6 ethanal (acetaldehyde)...11 ethyl acetate...11 ethyl carbamate...11 fatty acids...12 fish...1, 3, 4, 5, 10, 12 fish identification...3 fish muscle...4 fish oil...12 fish paste...1 fluoroquinolones...4 food simulant...6 fructose...2, 11 fruit juice...10 fruit purée...9 fumonisins...8 ginger (spice)...7 glucose...2, 11 gluten...5 grape purée...15 grapefruit juice...11 green bean purée...15 green coffee...8 ground coffee...11 hazelnut (water/nut slurry)...7 higher alcohols (sum)...11 histamine...5 honey...2, 4 hot pepper sauce...9 hydrogenated vegetable oil...13 hydroxymethylfurfural (HMF)...2 hydroxyproline...1 illegal dyes...9 immersion in ethanol...6 immersion in olive oil...6 infant cereal...10 infant formula...10, 12 infant soya formula...5 instant coffee...8 iodine...6, 12 iodine value...12 iron...5, 6, 10 jam...5, 9 k232 & k lactose...1 lamb...3 LCPUFAs...12 lead...5, 10 lettuce purée...3, 15 leucomalachite green...4 linoleic acid...12 liquid vitamin supplement...9 magesium...5 magnesium...5, 6, 11 maize...7 maize flour...8, 14 malachite green...4 manganese...5, 6 meat...3, 9 melamine...2, 6 mercury...10 mercury, methyl...10 methanol...11 methylbutanol...11 milk...5 milk powder...1, 2, 3, 6, 7, 9, 10, 13 mixed fat spread...12 mixed fruit drink...15 moisture...1, 2, 5 molybdenum...10 nitrate...3 nitrite...3 nitrofuran metabolites...4 nitrofurans...4 nitrogen...1 non-fat solids...1 non-permitted colours...9 NSAIDs...4 NSP fibre...1 nutritionally fortified oil...12 nylon film...6 oat flour...8 ochratoxin A...8 oil...6, 9

3 Oils & Fats...12 prawns...4 tea...15 oily fish...13 olive oil...6, 12, 13 omega-3 & omega orange juice...11 overall migration...6 PAHs...6 PAHs (EU priority)...6 palm oil...6 paprika...8 patulin...7 peanut...5, 7 peanut, peanut protein...5 pear purée...15 permitted colours...9 peroxide value...12 pesticide residues...13, 14, 15, 16 ph...9, 11 phosphoric acid (as P2O5)...11 phosphorus...5, 6, 11 phthlates...6 pig kidney...4 pig liver...4 pig ration...5 pistachio (water/nut slurry)...7 plastic film...6 polyphosphates...1 pork...3 porridge oats...1 potassium...6, 11 potato purée...15 poultry ration...5 powdered baby food...9 powdered rice...10 premix...5 protein...5 quinine...11 quinolones...4 quinolones & fluoroquinolones...4 refined palm oil...2 rice...3, 7 rice (brown)...14 roasted coffee...8 saccharin...11 saturated FAs...12 selenium...5, 6, 10 sheep feed...5 smoked meat...6 snack food...1 sodium...1, 5, 6, 9, 11 soft drink...10, 11 sorbic acid...9, 11 soy sauce...2 soya flour...10 soya, soya protein...5 spinach purée...3 starch...1, 5 strawberry purée...15 streptomycin...4 sucrose...1, 2, 9, 11 sugar confectionary...9 sulfonamides...4 sulphites...5 sulphur dioxide...9 sweet (bell) pepper purée...15 synthetic hormones...4 T-2 & HT-2 toxins...8 tequila...11 tetracyclines...4 theobromine...9 tin...10 titratable acidity...1 tomato paste...10 tomato purée...15 tomato sauce...9 tonic water...11 total acidity...9, 11 total dietary fibre...1 total fat...1, 12 total folate...9 total niacin...9 total oil...5 total primary aromatic amines...6 total SO total sugars...1, 5, 9, 11 total volatile basic nitrogen (TVB-N)..1 trans fatty acids...12 unsaturated FAs, mono...12 unsaturated FAs, poly...12 vegetable oil...12 vegetable purée...10 vitamins...5, 9 volatile acidity...11 wheat flour...1, 5, 8, 14 whisky...11 wine...8, 10, 11, 15 zearalenone (ZON)...8 zinc...5, 6, 10 lemon purée...15 β-agonists...4

4 Besin Bileşenleri 08/04/ canned meat moisture, ash, total fat, nitrogen, sodium & chloride 04/05/ canned meat meal moisture, ash, total fat, nitrogen, sodium & chloride 01/06/ canned meat moisture, ash, total fat, nitrogen, hydroxyproline 26/08/ canned meat moisture, ash, total fat, nitrogen, hydroxyproline 01/12/ canned meat meal moisture, ash, total fat, nitrogen, sodium, chloride, total sugars 15/02/ canned meat moisture, ash, total fat, nitrogen, sodium, chloride & polyphosphates 28/04/ wheat flour moisture at 130 C, ash, nitrogen & total dietary fibre by AOAC 08/06/ porridge oats moisture at 130 C, ash, total fat, nitrogen, total dietary fibre by AOAC & NSP fibre by Englyst 29/09/ cereal moisture at 130 o C, ash, nitrogen & total dietary fibre by AOAC 19/01/ breadcrumbs moisture, ash, nitrogen, starch & total dietary fibre by AOAC 25/05/ corn/maize snack food moisture, ash, total fat, nitrogen, sodium & chloride 24/06/ fish paste moisture, ash, total fat, nitrogen, sodium & chloride 19/08/ condensed milk moisture, ash, total fat, nitrogen & total sugars ml 23/09/ canned fish total volatile basic nitrogen (TVB-N) 1 17/10/ chocolate moisture, total fat, butyric acid, lactose & sucrose 03/01/ milk powder moisture, ash, total fat, nitrogen, titratable acidity & lactose 06/02/ butter moisture, total fat, non-fat solids, ph & chloride 07/03/ cheese & pasta meal moisture, ash, total fat, nitrogen, sodium & chloride Dipnotlar total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa, fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı g 100 g 1

5 FAPAS YETERLİK TESTLERİ PROGRAMI Acrylamide / Melamine / 3-MCPD 27/04/ crispbread acrylamide 12/08/ milk powder melamine & cyanuric acid (low levels, <5 mg/kg) 20/10/ biscuits acrylamide 16/02/ milk powder melamine and cyanuric acid (> 5mg/kg) 27/05/ soy sauce 3-MCPD & 1,3 DCP 40 g 21/09/ refined palm oil esters of 3-MCPD 50 ml 08/02/ soy sauce 3-MCPD & 1,3 DCP 40 g Honey 14/06/ honey moisture, fructose, glucose, sucrose, hydroxymethylfurfural (HMF) & diastase 22/11/ honey a moisture, fructose, glucose, sucrose, hydroxymethylfurfural (HMF) & diastase 100 g 100 g Dipnotlar a bu test materyali tağşişli bal olabilir 2

6 Authenticity 13/04/ D chicken contamination (presence/absence) of matrix with one or more from: beef, lamb or pork 25/05/ R rice identification of EU approved Basmati rice types and identification and quantification of EU non-approved Basmati rice types 22/07/ D lamb contamination (presence/absence) of matrix with one or more from: beef, chicken or pork 27/09/ fish identification of unknown fish (3 samples) selected from the following list: Gadus morhua, (Linnaeus 1758) Limanda limanda, (Linnaeus 1758) Melanogrammus aeglefinus, (Linnaeus 1758) Merluccius merluccius, (Linnaeus 1758) Hippoglossus hippoglossus, (Linnaeus 1758) Pleuronectes platessa, (Linnaeus 1758) Pollachius virens, (Linnaeus 1758) Merlangius merlangus, (Linnaeus 1758) 02/12/ D beef contamination (presence/absence) of matrix with one or more from: chicken, lamb or pork 30 g 2 x 10 g 30 g 3 x 10 g 30 g Nitrate & Nitrite 26/04/ cabbage purée nitrate 70 g 30/06/ φ meat nitrate & nitrite 25 g 15/08/ lettuce purée nitrate 70 g 19/10/ φ milk powder nitrate & nitrite (low level) 40 g 30/11/ φ meat nitrate & nitrite 25 g 24/01/ spinach purée nitrate 70 g 28/03/ φ meat nitrate & nitrite 25 g Dipnotlar R test Basmati Rice numunelerinin AB düzenlemelerine uygunluğunun/uygunsuzluğunun tespitine yöneliktir D dondurarak kurutulmuş (freeze dried) numune, analizden önce tekrar sulandırılmalıdır. φ testin süresi kısadır 3

7 Veteriner İlaç Kalıntıları 12/04/ honey streptomycin & dihydrostreptomycin 20 g 03/05/ φ prawns chloramphenicol 20 g 17/05/ φ# fish muscle tetracyclines 20 g 21/06/ φ# prawns nitrofuran metabolites 20 g 05/07/ φ fish muscle malachite green, leucomalachite green, total malachite green 20 g 08/08/ φ# pig kidney sulfonamides 20 g 22/08/ φ# fish muscle quinolones & fluoroquinolones 20 g 20/09/ φ# corned beef avermectins 20 g 04/10/ φ# pig liver β-agonists 20 g 25/10/ honey chloramphenicol 20 g 01/11/ φ# bovine kidney tetracyclines 20 g 29/11/ φ# chicken eggs nitrofuran metabolites 20 g 13/12/ φ fish muscle (oily fish) malachite green leucomalachite green, total malachite green 17/01/ # honey sulfonamides 20 g 07/02/ # bovine milk (milk powder) 28/02/ # chicken egg (whole egg powder) NSAIDs (nonsteroidal anti-inflammatory drugs) coccidiostats 20/03/ φ# bovine urine synthetic hormones 25 ml Testlerde belirtilen genel kategorilerdeki muhtemel ilaç kalıntılarının listesi - Liste A. tetracyclines chlortetracycline (total), doxycycline, oxytetracycline (total), tetracycline (total) nitrofurans AHD (bound), AHD (total), AOZ (bound), AOZ (total), AMOZ (bound), AMOZ (total), SEM (bound), SEM (total) sulfonamides sulfachloropyridazine, sulfadiazine, sulfadimethoxine, sulfadimidine (sulfamethazine), sulfadoxine, sulfaguanadine, sulfamerazine, sulfamethizole, sulfamethoxazole, sulfamethoxypyridazine, sulfamonomethoxine, sulfamoxole, sulphanilamide, sulfapyridine, sulfaquinoxaline, sulfathiazole, sulfisoxazole quinolones & fluoroquinolones flumequine, nalidixic acid, oxolinic acid, ciprofloxacin, danofloxacin, difloxacin, enrofloxacin, marbofloxacin, norfloxacin, sarafloxacin avermectins abamectin, doramectin, emamectin, eprinomectin, ivermectin, moxidectin β-agonists bromobuterol, cimaterol, cimbuterol, clenbuterol, clenpenterol, hydroxyclenbuterol, mabuterol, mapenterol, ractopamine, salbutamol, salmeterol, terbutaline, tulobuterol, zilpaterol synthetic hormones α-boldenone, methylboldenone, diethylstilbestrol (DES), dienestrol, hexoestrol, methyltestosterone, α-nortestosterone, stanozolol, 16β-hydroxystanozolol, trenbolone, zeranol nonsteroidal anti-inflammatory drugs diclofenac, 5-hydroxyflunixin, ibuprofen, meloxicam, naproxen, phenylbutazone (NSAIDs) ) coccidiostats diclazuril, lasalocid, maduramycin, monensin, narasin, nicarbazin (as 4,4-dinitrocarbanilide), salinomycin Dipnotlar # test Liste A'da belirtilen analitlerin belirlenmesi ve miktar tayinlerini içerir. φ testin süresi kısadır. 20 g 20 g 20 g 4

8 Yem Maddeleri 19/05/ dairy ration moisture, ash, total oil, protein & crude fibre 1 19/05/ dairy ration iron, lead, magnesium, manganese & selenium 1 16/06/ sheep feed moisture, ash, total oil, protein & copper 1 06/10/ pig ration moisture, ash, total oil, protein, crude fibre, vitamin E & zinc 1 24/11/ poultry ration moisture, ash, total oil, protein & crude fibre 1 24/11/ poultry ration starch, total sugars, calcium & phosphorus 1 09/02/ premix calcium, manganese, magnesium, phosphorus, sodium & zinc 1 09/02/ premix vitamin A, D 3, E 1 Allerjenler Histamin ve sülfitler DIŞINDA (genellikle HPLC metotları kullanılır), sonuçlar ELISA kitlerinin markasına göre gruplandırılarak değerlendirilir. 13/04/ infant soya formula casein 2 x 20 g 04/05/ canned fish histamine (high level) 145 g 08/06/ cake mix egg, egg white protein 2 x 20 g 30/06/ infant soya formula gluten 2 x 20 g 21/07/ chocolate peanut, peanut protein 2 x 20 g 04/08/ infant soya formula beta-lactoglobulin 2 x 20 g 24/08/ cake mix gluten 2 x 20 g 01/09/ canned fish histamine (low level) 145 g 21/09/ chocolate hazelnut, hazelnut protein 2 x 20 g 18/10/ jam sulphites 20 g 02/11/ cake mix gluten, milk and egg 30 g 04/01/ wheat flour soya, soya protein 2 x 20 g 17/02/ canned fish histamine (high level) 145 g 01/03/ chocolate almond, almond protein 2 x 20 g Dipnotlar total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa, fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı. iki adet test materyali gönderilir. Kalitatif ve kantitatif sonuçlar bildirilebilir. Kalitatif ve kantitatif sonuçlar bildirilebilir. 5

9 Çevresel Bulaşanlar 20/04/ palm oil PAHs 30 ml 20/09/ smoked meat product PAHs 05/01/ olive oil all 16 EU priority PAHs 30 ml Migrasyon Overall & Specific 20/04/ nylon film overall migration into ethanol by total immersion 03/11/ plastic film overall migration into olive oil by total immersion 40 cm x 22 cm 40 cm x 22 cm 29/06/ B food simulant phthalates 2 x 50 ml 17/08/ % w/v acetic acid in water melamine 1 x 50 ml 07/09/ B food simulant bisphenol A 2 x 50 ml 17/11/ food simulant total primary aromatic amines >300 ml 08/03/ oil photo initiators >50 ml Besin Elementleri 07/04/ canned meat calcium, phosphorus & zinc (all natural levels) 1 14/07/ breakfast cereal calcium, iron & zinc (fortified) 10/08/ bread sodium 16/11/ milk powder calcium, iodine & selenium, (all natural levels) 23/03/ energy drink iron, magnesium, manganese, potassium, selenium, (all natural levels) Dipnotlar B Blank matriks dahildir. 6

10 Mikotoksinler Aflatoxins ve ELISA taramaları yapan laboratuvarlara yöneliktir. 19/04/ pistachio (water/nut slurry) aflatoxins B & G &/or total 100 g 27/04/ maize aflatoxins B & G &/or total 55 g 12/05/ milk powder aflatoxin M 1 55 g 16/06/ maize aflatoxin B 1, DON, ZON & OTA 1 06/07/ chilli powder aflatoxins B & G &/or total 55 g 28/07/ animal feed (cereal based) aflatoxins B & G &/or total 55 g 31/08/ maize aflatoxins B & G &/or total 55 g 08/09/ milk powder aflatoxin M 1 55 g 15/09/ maize aflatoxin B 1, DON, ZON & OTA 1 26/09/ hazelnut (water/nut slurry) 10/10/ almond (water/nut slurry) aflatoxins B & G &/or total aflatoxins B & G &/or total 100 g 100 g 02/11/ peanut aflatoxins B & G &/or total 55 g 23/11/ ginger (spice) aflatoxins B & G &/or total 55 g 06/01/ animal feed (cereal based) 31/01/ pistachio (water/nut slurry) aflatoxins B & G &/or total aflatoxins B & G &/or total 55 g 100 g 08/02/ rice aflatoxins B & G &/or total 55 g 29/02/ peanut aflatoxins B & G &/or total 55 g 12/03/ dried figs (water/fruit slurry) aflatoxins B & G &/or total 100 g 22/03/ milk powder aflatoxin M 1 55 g Mikotoksinler Patulin 13/06/ apple juice (clear) patulin 50 ml 11/10/ apple purée patulin 60 g 27/03/ apple juice (cloudy) patulin 50 ml 7

11 Mikotoksinler Okratoksin A 05/05/ maize flour ochratoxin A 55 g 20/06/ dried vine fruit (water/fruit slurry) ochratoxin A 100 g 08/07/ barley flour ochratoxin A 55 g 11/08/ green coffee ochratoxin A 55 g 09/09/ paprika ochratoxin A 55 g 27/10/ instant coffee ochratoxin A 55 g 07/12/ wine ochratoxin A 55 ml 10/01/ wheat flour ochratoxin A 55 g 02/02/ roasted coffee ochratoxin A 55 g 02/03/ animal feed ochratoxin A 55 g 29/03/ cocoa ochratoxin A 55 g Mikotoksinler Fusarium toksinleri 07/04/ maize flour deoxynivalenol (DON) 55 g 12/05/ maize flour FB 1 & FB 2 (not total fumonisins) 55 g 13/07/ animal feed zearalenone (ZON) 55 g 02/08/ animal feed deoxynivalenol (DON) 55 g 30/08/ breakfast cereal zearalenone (ZON) 55 g 26/10/ breakfast cereal deoxynivalenol (DON) 55 g 12/01/ oat flour T-2 & HT-2 toxins 55 g 10/02/ wheat flour deoxynivalenol (DON) 55 g 15/03/ animal feed T-2 & HT-2 toxins 55 g 8

12 Vitaminler 26/05/ φ fruit purée vitamin C 100 ml 15/07/ breakfast cereal vitamins B 1, B 2 (total) & B 6, total niacin & total folate 15/11/ liquid vitamin supplement vitamins B 1, B 2 (total) & B 6 40 ml 25/01/ milk powder vitamins A & D 3 14/03/ powdered baby food Gıda Katkı Maddeleri vitamins A, B 12, C & E 06/04/ tomato sauce brix, ph, total acidity, sodium & chloride 1 10/05/ meat sulphur dioxide 100 g 22/06/ jam brix, ph, benzoic acid, citric acid & sorbic acid 16/08/ chocolate cake mix 13/09/ dried apricot (water/fruit slurry) 19/10/ sugar confectionary (boiled sweets) caffeine, sorbic acid, theobromine & total sugars (expressed as sucrose) sulphur dioxide permitted colours up to 4 selected from the following list: Allura Red, Brilliant Blue FCF, Carmoisine, Erythrosine, Green S, Indigo Carmine, Patent Blue V, Ponceau 4R, Quinoline Yellow, Sunset Yellow FCF, Tartrazine 08/12/ oil antioxidants: total BHA (E320), BHT (E321) & propyl gallate (E310) 01/02/ hot pepper sauce (or similar) non-permitted colours (illegal dyes) up to 4 selected from the following list: Butter Yellow (Dimethyl Yellow), Orange II, Para Red, Rhodamine B, Sudan I, Sudan II, Sudan III, Sudan IV, Sudan Black B, Sudan Orange G, Sudan Red B, Sudan Red 7B, Sudan Red G, Toluidine Red 100 g 50 ml 50 ml Dipnotlar total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa, fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı. φ testin süresi kısadır. Kalitatif ve kantitatif sonuçlar bildirilebilir. 9

13 Metalik Bulaşanlar 14/04/ milk powder arsenic, cadmium, (natural levels), mercury, lead, (high levels) 11/05/ soft drink antimony, arsenic (total) cadmium, chromium copper & zinc (all high levels) 15/06/ canned fish arsenic (total), lead, cadmium & mercury (total) (all natural levels) 50 ml 1 28/06/ tomato paste cadmium, lead, iron & tin (all high levels) 20/07/ chilli powder arsenic (total), cadmium & lead (all high levels) 03/08/ infant formula aluminium, chromium, molybdenum, selenium (all low levels) 25/08/ canned crab meat arsenic (total), arsenic (inorganic), cadmium, lead & mercury (total), (all natural levels) 1 14/09/ chilli sugar paste lead 25 g 28/09/ edible oil arsenic (total), copper, iron & lead (all high levels) 50 ml 05/10/ wine ph, cadmium & lead 100 ml 26/10/ canned fish arsenic (total), cadmium, mercury (total) (all natural levels) 10/11/ infant cereal cadmium, chromium, lead, mercury (total), selenium (all natural levels) 01/12/ soya flour aluminium, arsenic (total), cadmium, lead & mercury (total) (all high levels) 13/01/ cocoa powder cadmium & lead (both natural levels) 1 14/02/ fruit juice cadmium, iron, lead, & tin (all high levels) 50 ml 24/02/ powdered rice arsenic (inorganic), arsenic (total) & cadmium (all high levels) 13/03/ vegetable purée cadmium, lead & tin (all high levels) 21/03/ canned fish arsenic (total), methyl mercury & mercury (total) (all natural levels) 1 10

14 Meyve Suyu, Alkollü ve Alkolsüz İçecekler 09/06/ apple juice brix, ph, total acidity, total sugars, magnesium, potassium & sodium 14/10/ orange juice brix, ph, citric acid, sucrose, glucose, fructose & total sugars 26/01/ grapefruit juice brix, ph, total acidity, total sugars, calcium, magnesium & potassium 16/03/ cranberry juice brix, ph, total acidity, total sugars, phosphorus & potassium 13/05/ cola drink benzoic acid, caffeine, acesulfame-k & saccharin 14/07/ ground coffee caffeine (2 test materials supplied, one regular, one decaffeinated) 23/08/ soft drink brix, ph, citric acid, sorbic acid, cyclamate & saccharin 13/10/ soft drink up to 4 colours from the following list: Allura Red, Brilliant Blue FCF, Carmoisine, Erythrosine, Green S, Indigo Carmine, Patent Blue V, Ponceau 4R, Quinoline Yellow, Sunset Yellow FCF, Tartrazine 09/12/ cola drink caffeine, benzoic acid, total sugars & phosphoric acid (as P 2O 5) 18/01/ tonic water benzoic acid, quinine, acesulfame-k & aspartame 18/05/ whisky alcoholic strength, ethanal (acetaldehyde), ethyl acetate, methanol, propan-1-ol, 2-methylpropanol & 2-methylbutanol + 3-methylbutanol (sum) 08/09/ brandy alcoholic strength, ethanal (acetaldehyde), ethyl acetate, methanol, propan-1-ol, 2-methylpropanol & 2-methylbutanol + 3-methylbutanol (sum) & ethyl carbamate 16/11/ wine alcoholic strength, total SO 2, total acidity & volatile acidity 22/02/ tequila alcoholic strength, ethanal (acetaldehyde), ethyl acetate, methanol, propan-1-ol, 2-methylpropanol & 2-methylbutanol + 3-methylbutanol (sum) 250 ml 250 ml 250 ml 250 ml 150 ml 2 x 30 g 150 ml 150 ml 150 ml 150 ml 200 ml 200 ml 220 ml 200 ml Dipnotlar total sugars = titrasyon metodu sonucu (ör. Layne-Eynon, Luff-Schoorl, Munson Walker) veya HPLC ile yapıldıysa, fruktoz, glikoz, sakkaroz, laktoz, galaktoz ve maltoz toplamı. Kalitatif ve kantitatif sonuçlar bildirilebilir. 11

15 Yağlar FAPAS YETERLİK TESTLERİ PROGRAMI 26/04/ nutritionally fortified oil (may contain LC-PUFAs) 10/05/ infant formula (may contain LC-PUFAs) saturates, mono-unsaturates, poly-unsaturates, total trans fatty acids, linoleic acid, α-linolenic acid (ALA), ARA & DHA total fat, saturates, mono-unsaturates, poly-unsaturates, total trans fatty acids, linoleic acid, α-linolenic acid (ALA), ARA, & DHA 07/06/ φ olive oil peroxide value, acidity, anisidine value & iodine value 12/07/ cereal product (may contain LC-PUFAs) 19/07/ nutritionally fortified oil (may contain LC-PUFAs) total fat, saturates, mono-unsaturates, poly-unsaturates, total trans fatty acids, linoleic acid, α-linolenic acid (ALA), ARA, & DHA saturates, mono-unsaturates, poly-unsaturates, total trans fatty acids, linoleic acid, α-linolenic acid (ALA), ARA & DHA 15/08/ mixed fat spread total fat, saturates, mono-unsaturates, poly-unsaturates, & trans fatty acids 05/10/ φ olive oil peroxide value, acidity, anisidine value & iodine value 30 ml 100 ml 30 ml 100 ml 20/10/ fish oil omega-3 & omega-6 series fatty acids 30 ml 08/11/ mixed fat spread total fat, butyric acid & cholesterol 19/01/ vegetable oil saturates, mono-unsaturates, poly-unsaturates 30 ml 06/03/ φ olive oil peroxide value, acidity, K 232 & K ml Dipnotlar φ testin süresi kısadır. 12

16 Pestisit Kalıntıları Hayvansal Ürünler / Yağlar Her hest materyali Liste 1'de belirtilen pestisitlerden birkaç tanesini içerir. 21/04/ hydrogenated vegetable oil selection from List 1 25 g 0576b blank hydrogenated vegetable oil BLANK (only available if ordered with test 0576) 25 g 26/05/ milk powder selection from List 1 26/07/ olive oil selection from List 1 15/09/ hydrogenated vegetable oil selection from List 1 25 g 0579b blank hydrogenated vegetable oil BLANK (only available if ordered with test 0579) 25 g 14/11/ oily fish selection from List 1 21/02/ animal (pork) fat selection from List 1 Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) Liste 1 aldrin lambda-cyhalothrin fenthion methacrifos tecnazene azinphos-ethyl pp -DDE fenthion sulfone methidathion triazophos bifenthrin pp -DDD (TDE) fenthion sulfoxide 4,4 -methoxychlor vinclozolin cis-chlordane op -DDT fenvalerate nitrofen PCB 28 trans-chlordane pp -DDT formothion parathion-ethyl PCB 52 oxychlordane deltamethrin hexachlorobenzene (HCB) parathion-methyl PCB 101 chlorobenzilate diazinon alpha-hexachlorocyclohexane (α-hch) pendimethalin PCB 118 chlorfenvinphos dieldrin beta-hexachlorocyclohexane (β-hch) permethrin (sum isomers) PCB 138 chlorpyrifos (-ethyl) alpha-endosulfan (endosulfan I) gamma- hexachlorocyclohexane (lindane) pirimiphos-methyl PCB 153 chlorpyrifos-methyl beta-endosulfan (endosulfan II) heptachlor profenofos PCB 180 cyfluthrin (sum isomers) endosulfan sulfate cis-heptachlor epoxide pyrazophos cypermethrin endrin trans-heptachlor epoxide quintozene 13

17 Pestisit Kalıntıları Tahıl Ürünleri Her test materyali (0973 hariç) Liste 2'de belirtilen pestisitlerden birkaç tanesini içerir. 11/05/ maize flour selection from list 2 27/07/ wheat flour selection from list b blank wheat flour BLANK (only available if ordered with test 0972) 12/10/ cereal chlormequat (single pesticide) 09/11/ brown rice selection from List 2 23/02/ barley flour selection from list 2 Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) Liste 2 acephate deltamethrin fenvalerate (sum isomers) metconazole quinoxyfen azinphos-methyl demeton-s-methyl sulfone fipronil methacrifos quintozene azoxystrobin diazinon fludioxonil methomyl spiroxamine bifenthrin dichlorvos fluquinconazole metribuzin tebuconazole captan difenoconazole flusilazole omethoate tebufenozide carbaryl diflubenzuron flutriafol oxydemeton-methyl (demeton-s-methyl sulfoxide) thiabendazole carbendazim (sum of carbendazim, benomyl and thiophanatemethyl ) dimethoate formothion paclobutrazole thiacloprid carbofuran dimoxystrobin alpha-hexachlorocyclohexane (α-hch) 3-hydroxycarbofuran alpha-endosulfan (endosulfan I) beta-hexachlorocyclohexane (β-hch) parathion-ethyl penconazole thiamethoxam thiodicarb carboxin beta-endosulfan (endosulfan II) gamma-hch (lindane) pendimethalin triadimefon chlorfenvinphos endosulfan sulfate hexaconazole permethrin (sum) triadimenol chlorothalonil epoxiconazole imazalil phosmet triazophos chlorpropham ethion imidacloprid phosphamidon (sum isomers) tricyclazole chlorpyrifos etrimphos iprodione pirimicarb trifloxystrobin chlorpyrifos-methyl fenbuconazole isofenphos-methyl desmethyl-pirimicarb trifluralin clothianidin fenhexamid isoprothiolane pirimiphos-methyl triticonazole cyfluthrin (sum) fenitrothion isoproturon prochloraz vinclozolin cypermethrin fenpropimorph kresoxim-methyl procymidone cyproconazole fenthion linuron propiconazole cyprodinil fenthion sulfone malaoxon pyraclostrobin lambda-cyhalothrin fenthion sulfoxide malathion pyrimethanil 14

18 Pestisit Kalıntıları Taze Meyve ve Sebzeler & İçecekeler Meyve ve sebze matriksleri taze meyve ve sebzelerin püre haline getirilmesiyle hazırlanacaktır. Herbir test materyali (19129 hariç) Liste 3'te belirtilen pestisitlerden birkaçını içerir Liste 4'te belirtilen pestisitlerden birkaçını içerir. 14/04/ wine pesticide residues from List b blank wine BLANK (only available if ordered with test 19119) 18/04/ P apple pesticide residues from List b P blank apple BLANK (only available if ordered with test 19120) 23/05/ P lemon pesticide residues from List 3 90 ml 19121b P blank lemon BLANK 90 ml (only available if ordered with test 19121) 23/05/ mixed fruit drink (pasteurised) pesticide residues from List b blank mixed fruit drink BLANK (only available if ordered with test 19122) 19/09/ P tomato pesticide residues from List 3 90 ml 19123b P blank tomato BLANK 90 ml (only available if ordered with test 19123) 19/09/ P strawberry pesticide residues from List b P blank strawberry BLANK (only available if ordered with test 19124) 24/10/ P sweet (bell) pepper pesticide residues from List b P blank sweet (bell) pepper BLANK (only available if ordered with test 19125) 24/10/ P cherry pesticide residues from List b P blank cherry BLANK (only available if ordered with test 19126) 21/11/ P lettuce pesticide residues from List b P blank lettuce BLANK (only available if ordered with test 19127) 21/11/ P yard long bean (green bean with pods) pesticide residues from List P blank yard long bean (green bean with pods) BLANK (only available if ordered with test 19128) 11/01/ tea pesticide residues from List b blank tea BLANK (only available if ordered with test 19129) 23/01/ P pear pesticide residues from List b P blank pear BLANK (only available if ordered with test 19130) 27/02/ P grape pesticide residues from List b P blank grape BLANK (only available if ordered with test 19131) 27/02/ P potato pesticide residues from List b P blank potato BLANK (only available if ordered with test 19132) Dipnotlar P matriks püredir 15

19 Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) Liste 3 2-phenylphenol cyfluthrin (sum isomers) fenbuconazole methiocarb sulfone pyraclostrobin acephate lambda-cyhalothrin fenhexamid methiocarb sulfoxide pyrazophos acetamiprid cypermethrin (sum isomers) fenitrothion methomyl pyrethrins (sum) acrinathrin cyproconazole fenoxycarb 4,4 -methoxychlor pyridaben aldicarb cyprodinil fenpropathrin methoxyfenozide pyrimethanil aldicarb sulfone pp -DDD (TDE) fenpropimorph monocrotophos pyriproxyfen aldicarb sulfoxide pp -DDE fenvalerate (sum isomers) myclobutanil quinalphos amitraz op -DDT fipronil omethoate quinoxyfen atrazine pp -DDT fluazifop-p-butyl oxadixyl spinosad (spinosyn A + spinosyn D) azinphos-methyl deltamethrin fludioxonil oxamyl spiroxamine azoxystrobin demeton-s-methyl sulfone flufenoxuron oxydemeton-methyl tebuconazole (demeton-s-methyl sulfoxide) bifenthrin diazinon fluquinconazole oxyfluorfen tebufenozide bitertanol dichlofluanid flusilazole paclobutrazol tebufenpyrad boscalid dichlorvos flutriafol paraoxon-methyl tecnazene bromopropylate dicloran folpet parathion (-ethyl) teflubenzuron bromuconazole (sum) dicofol formetanate HCl parathion-methyl tefluthrin bupirimate dicrotophos fosthiazate penconazole tetraconazole buprofezin difenoconazole hexaconazole pencycuron tetradifon cadusafos dimethoate hexythiazox pendimethalin thiabendazole carbaryl dimethomorph (sum) imazalil permethrin (sum isomers) thiacloprid carbendazim (sum of diniconazole imidacloprid phenthoate thiamethoxam carbendazim, benomyl & thiophanate-methyl) carbofuran diphenylamine indoxacarb (sum isomers) phosalone thiodicarb 3-hydroxy carbofuran DMST iprodione phosmet tolclofos-methyl chlorfenapyr alpha-endosulfan (endosulfan I) iprovalicarb phoxim tolylfluanid chlorfenvinphos (sum beta-endosulfan (endosulfan II) kresoxim-methyl pirimicarb triadimefon isomers) chlormequat endosulfan sulfate lenacil desmethyl-pirimicarb triazophos (pear and grapes only) chlorobenzilate epoxyconazole linuron pirimiphos-methyl trifloxystrobin chlorthal-dimethyl ethion lufenuron prochloraz trifluralin chlorothalonil ethoprophos mepanipyrim procymidone triticonazole chlorpropham etofenprox metaflumizone profenofos vinclozolin chlorpyrifos (-ethyl) fenamiphos metalaxyl propamocarb zoxamide chlorpyrifos-methyl fenamiphos sulfone metconazole propargite chlozolinate fenamiphos sulfoxide methamidophos propiconazole clofentezine fenarimol methidathion propyzamide clothianidin fenazaquin methiocarb prothiofos Potansiyel pestisit kalıntıları (belirtilmediği sürece sadece ana madde) Liste 4 bifenthrin dicofol pp -DDT fenazaquin phosalone chlorothalonil dimethoate alpha-endosulfan (endosulfan I) fenitrothion procymidone chlorpyrifos (-ethyl) pp -DDD (TDE) beta-endosulfan (endosulfan II) fenpropathrin propargite lambda-cyhalothrin pp -DDE endosulfan sulfate fenvalerate (sum isomers) quinalphos cypermethrin (sum isomers) op -DDT ethion HCB (hexachlorobenzene) trifloxystrobin deltamethrin 16

20 İptal Şartları Testin dağıtım tarihine bir aydan daha kısa süre kaldığında iptali istenirse geri ödeme yapılmaz. Dağıtıma bir aydan daha fazla süre varsa test ücretinin %50'si iade edilir veya başka bir testle değiştirilebilir. Faturalandırma & Ödemeler Siparişleriniz bize ulaştığında yeterlik testlerine kayıt bedeli olarak tarafımızdan hizmet faturası düzenlenir. Numunelerin dağıtıımı belirtilen tarihlerde Food and Environment Research Agency tarafından yapılacağından, Sincer Dış Ticaret tarafından bir ürün teslimatı söz konusu değildir. Yeterlik testleri için numuneler belirtilen tarihlerde FERA tarafından DHL ile doğrudan tarafınıza gönderilecektir. Zaman zaman gümrük kontrolleri nedeni ile numunelerin gümrüklerde işlem görmesi olasıdır. Bu durumda numuneler ile ilgili gümrük işlemlerinin tarafınızca yürütülmesi gerekeceğini tekrar hatırlatırız. Ziya Gökalp Bul. 17/4 Alsancak, İzmir Tel: Faks: